Transcription of 1/2000
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1/2000
Interpreting DSC curvesPart 1: Dynamic measurementsThe art of interpreting curves has yet to be integrated into commercially available com-puter programs. The interpretation of a DSC measurement curve is therefore still some-thing you have to do yourself. It requires a considerable amount of experience in thermalanalysis as well as a knowledge of the possible reactions that your particular sample article presents tips and information that should help you with the systematic inter-pretation of DSC artifactsThe first thing to do is to examine the curve for any obvious artifacts that could lead to apossible misinterpretation of the results.
1) Samples of irregular form can topple over in the pan. 2) Polymer films that have not been pressed against the base of the pan first change shape (no longer lie flat) on initial warming. Afterward, on melting, they make good contact with the pan (Fig. 2). b)An abrupt change of the heat transfer between the pan and the DSC sensor:
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