Transcription of 1/2000 - University of Cincinnati
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1/2000 - University of Cincinnati
Interpreting DSC curvesPart 1: Dynamic measurementsThe art of interpreting curves has yet to be integrated into commercially available com-puter programs. The interpretation of a DSC measurement curve is therefore still some-thing you have to do yourself. It requires a considerable amount of experience in thermalanalysis as well as a knowledge of the possible reactions that your particular sample article presents tips and information that should help you with the systematic inter-pretation of DSC artifactsThe first thing to do is to examine the curve for any obvious artifacts that could lead to apossible misinterpretation of the results. Artifacts are effects that are not caused by thesample under investigation.
METTLER TOLEDO we call this "off-line thermogravimetry"). The best way is to measure a new sample in a TGA, ands use the same type of pan as for the DSC mea-surement. The shape of the DSC curve is usually very characteristic and helps to identify the na-ture of the effect. In the following sections, examples of the most important effects and ...
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