Transcription of AOAC Guidelines for Single Laboratory
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AOAC Guidelines for Single Laboratory
aoac Guidelines for Single Laboratory Validation of Chemical Methods for Dietary Supplements and Botanicals CONTENTS. Introduction Definitions Validation Method of analysis Performance characteristics of a method of analysis Single - Laboratory Validation Work Preparation of the Laboratory Sample Identification Method of Analysis or Protocol Optimization Reference standard Ruggedness Trial Specific variables a. Analyte addition b. Reextraction of the extracted residue c. Comparison with different solvents d. Comparison with results from a different procedure e. System Suitability Checks Performance Characteristics Applicability Selectivity Calibration External Standard Method Internal Standard Method Standard Addition Method Reliability Characteristics Accuracy Repeatability Precision (sr, RSDr). Measurement Uncertainty Reproducibility Precision (sR, RSDR). Intermediate Precision Limit of Determination Reporting Low-level Values Dichotomous Reporting Controls Control Charts Injection Controls Duplicate Controls Confirmation of Analyte 1 2002-12-19.
AOAC Guidelines for Single Laboratory Validation of Chemical Methods for Dietary Supplements and Botanicals CONTENTS 1.0 Introduction 1.1 Definitions
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