Transcription of Chapter 5 TGA Analysis & Thermal Conductivity - …
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Chapter 5 TGA Analysis & Thermal Conductivity - …
Chapter 5 TGA Analysis & Thermal Conductivity Chapter 5. TGA Analysis & Thermal Conductivity Introduction The Thermal methods usually employed are differential scanning calorimetry (DSC), differential Thermal Analysis (DTA), Thermogravimetric Analysis (TGA) and derivatographic Analysis . For comparative study of Thermal behavior of related polymer or simple molecules, each molecule is analyzed by any one or more of these methods of Analysis under identical experimental condition. For example TGA is carried out in air and in oxygen free nitrogen[1-3]. It is carried out at different heating rates. It may be method that the result of Thermal Analysis of a given sample by a given method depends on various aspects. The amount and particle size of the material being examined, influence the nature of the thermogram[4]. The speed of the recorder noting the change in weight and the shape of the sample container also influence the thermogravimetric results. The rate of heating the sample and the ambient atmosphere during Analysis are very important factors to be controlled during Thermal Analysis .
Chapter 5 TGA Analysis & Thermal Conductivity 122 | P a g e about the purity of the sample, as well as its water, carbonate and organic content.
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