Transcription of “Chiral Impurity Methods –Case Study” - HPLC
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“Chiral Impurity Methods –Case Study” - HPLC
chiral Impurity Methods case study Ch. LAKSHMI NARAYANADAICEL chiral TECHNOLOGIES (INDIA) PVT LTDIPCIPC--USPUSP8th8thASM 2009 ASM 2009 Introduction: chiral Impurity Methods Types of chiral Stationary Phases (CSPs) for HPLCP olysaccharide-CSPs Coated CSPs immobilised CSPs case study : Oxaliplatin chiral HPLC method Lamivudine chiral HPLC method Clopidogrel Bisulphate chiral HPLC methodOverviewOverviewChiral Impurity Methods chiral Impurity Methods IntroductionIntroduction chiral GC chiral HPLC chiral HPCE chiral SFCT ypes of CSPs and their loading capacitiesTypes of CSPs and their loading capacitiesDrug discovery today, volume 10, Number 8, April 2005 TypeCSPsLoading capacity(mg solute / g CSP)IPirkle type (Brush type)1-50 IIPolysaccharide derivatives5 150 IIIM acrocyclic Crown Impurity Methods chiral Impurity Methods Types of CSPT ypes of CSP1999200120032005 Polysaccharide80 5%3%12%87 4%2%7%86 2%1%11%92 4%2% 2%1995-2003 Tetrahedron Asymmetry2005 : J.
Introduction: Chiral Impurity methods Types of Chiral Stationary Phases (CSPs) for HPLC Polysaccharide-CSPs • Coated CSPs • immobilised CSPs Case study: • Oxaliplatin Chiral HPLC method • Lamivudine Chiral HPLC method • Clopidogrel Bisulphate Chiral HPLC method Overview
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