“Cooking with Chemicals” - MMS Conferencing

EYP 2006 EYP 2006 Differential Scanning Differential Scanning CalorimetryCalorimetryClare RawlinsonClare RawlinsonSchool of PharmacySchool of PharmacyUniversity of BradfordUniversity of Bradford cooking with ChemicalsCooking with Chemicals EYP 2006 EYP 2006 OutlineOutline brief history of thermal analysisBrief history of thermal analysis Theory of thermal analysis techniques Theory of thermal analysis techniques Thermal Gravimetric Analysis (TGA)Thermal Gravimetric Analysis (TGA) Differential Scanning Calorimetry (DSC)Differential Scanning Calorimetry (DSC) Generating valid dataGenerating valid data CalibrationCalibration Sample preparationSample preparation Interpreting data and ApplicationsInterpreting data and Applications Real eventsReal events ArtefactsArtefacts Recent advancesRecent advancesEYP 2006 EYP 2006 CalorimetryCalorimetry CalorimetryCalorimetry The study of heat transfer during The study of heat transfer during physical and chemical processesphysical and chemical processes CalorimeterCalorimeter A device for measuring the heat A device for measuring the heat transferredtransferredLavoisierLavoisier and and LaplaceLaplace(1782(1782--1784):1784): oil was burned in a lamp (oil was burned in a lamp (Fig 9 Fig 9) held in ) held in a bucket (Fig.)

EYP 2006 Outline Brief history of thermal analysis Theory of thermal analysis techniques – Thermal Gravimetric Analysis (TGA) – Differential Scanning Calorimetry (DSC) GenerGenerating valid dataating valid data – Calibration – Sample preparation

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