Transcription of GC MS, LC 誘導体化 - jsac.or.jp
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GC MS, LC 誘導体化 - jsac.or.jp
GC/MS, LC/MS .. UV VIS FL .. / LC/MS .. GC/MS, LC/MS .. 1 GC/MS 1)2).. 1 1 .. ECD F, .. Cl, Br, I .. ECD .. GC/MS .. / GC / MS .. GC/MS .. 10 .. 11 NICI . Fundamental Knowledge of Chemical Analysis Derivatization . for GC/MS, LC/MS.. 12 . 332 . 1) 3).. 13 .. GC/MS .. GC/MS . 1 2 . GC/MS I .. 1 . TMS TMSI . BSTFA BSA MSTFA TMSDMA TMSDEA . MTMSA TMCS HMDS .. 1 2 3 . 1 2 . 1 . 333. II .. t BDMS M GC/ MS . t . t . TMCS M C(CH3 )3] M 57] .. SIM . BSA TMSI TMCS 1 1 1 . TMS . t BDMS . MTBSTFA 1 t BDMCS . t . BDMCS .. 100 . C .. NH2 OH . SH . DMF THF . DMSO N . MBTFA . GC/MS . GC / MS TFAA . TMS TMS TMS CH3 )3 Si ] PFPA . EI HFBA . m / z m 2 . z 73 . TMS EI GC/MS .. TMS ECD .. 2 . TMS .. TMS GC / MS . tert t . BDMCS N N tert . MTBSTFA . t BDMCS . tert t . BDMS MTBSTFA 5 . 20 t BDMS . 334 . ECD . NICI .. 2 .. III .. LC/MS . GC .. 1 3 GC/MS .. 2 2 . LC/MS.
334 ぶんせき 表2 主な無水フルオロアシル化剤 使用の際は，火気厳禁で換気のよい場所で作業する。
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