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Guide to Holding Times, Containers, and Preservatives ...

ParameterEPA Method(s)MinimumVolumeContainerTypeRequi redPreservativeHolding TimeContainerTypeRequiredPreservativeHol ding TimeDGAS - Methane, Ethane, Ethene, CO2 RSK SOP 175/147 3 X 40 mLVOA VialsIce7 / 14 Days CO2 only DGAS - Methane, Ethane, Ethene (w/o CO2)RSK SOP 175/147 3 X 40 mLVOA VialsHCl to pH<2 / Ice14 Days Explosives8330A 2 X 500 mLAmber GlassIce7E / 40A (Days)8 oz glass jarIce14E / 40A (Days)Glycols8015D 500 mLHDPE/GlassIce7E / 40A (Days)4 oz glass jarIce14E / 40A (Days)Herbicides8321B 500 mLAmber GlassIce7E / 40A (Days)4 oz glass jarIce14E / 40A (Days)PAH - Polynuclear Aromatic Hydrocarbons625/8270D 2 X 500 mLAmber GlassIce7E / 40A (Days)4 oz glass jarIce14E / 40A (Days)Pesticides - Organochlorine andOrganophosphorus608/625/8270D 2 X 500 mLAmber GlassIce7E / 40A (Days)4 oz glass jarIce14E / 40A (Days)PCBs/Aroclors - Polychlorinated Biphenyls608/625/8082/8270 2 X 500 mLAmber GlassIce7E / 40A (Days)4 oz glass jarIce14E / 40A (Days)SVOC - Semi-Volatile Organics (BNA)625/8270D 2 X 500 mLAmber GlassIce7E / 40A (Days)4 oz glass jarIce14E / 40A (Days)TPH - Total Petroleum HydrocarbonsTX 1005 3 X 40 mLVOA VialsHCl to pH<2 / Ice14 Days4 oz glass jarIce14 DaysTPH - Fractionation by TX 1006TX 1006 3 X 40 mLVOA VialsHCl to pH<2 / Ice14 Days after 1005E4 oz glass j

TPH-DRO - Diesel Range Organics 8015D 2 X 500 mL Amber Glass HCl to pH<2 / Ice 7E / 40A (D ays) 4 oz glass jar Ice 14E / 40A (D ays) Method 5035 Prep (BTEX-MTBE, GRO, VOC) 5035 ── ── ── ── 3 tared VOA Vials Ice **Ship ASAP**

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