Transcription of Instrument Configuration for Powder Diffraction
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Instrument Configuration for Powder Diffraction
Advanced X ray Bose National Centre for Basic Sciences, 14 15/12/2011 Instrument Configuration for PowderDiffractionInnovation with Integrity What is the application? What are the requirements of your application? Early decisions: What are the sample properties? What data quality is necessary? What Instrument and measurement parameters to use?Advanced X ray Workshop2 OverviewSampleInstrumentDataCollectionEa rly Decisions14 15/12/ 2011"Although the physical nature of a specimen from which the X ray Powder Diffraction data are collected is seemingly simple, sample preparation and data collection are generally the source of most of the serious problems with accurate X ray Diffraction analysis" Too small number of scattering particles / coarse grains (spotiness) Preferred orientation Inappropriate Instrument geometry / sample presentation Unsuited step
Advanced X-ray Workshop S.N. Bose National Centre for Basic Sciences, 14-15/12/2011 Instrument Configuration for Powder Diffraction Innovation with Integrity
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