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LA ABBOORRAATTO ORRYY MMANNUUAALL …

CHE 1401 Last update: June 2011 1 SScchhooooll ooff SScciieennccee && EEnnggiinneeeerriinngg LLAABBOORRAATTOORRYY MMAANNUUAALL FFOORR OORRGGAANNIICC CCHHEEMMIISSTTRRYY II Last Update: July 2015 CHE 2401 Last update: June 2011 1 Name: _____ Section: _____ LLAABBOORRAATTOORRYY MMAANNUUAALL FFOORR OORRGGAANNIICC CCHHEEMMIISSTTRRYY II Last Update: July 2015 CHE 2401 lab manual i TTAABBLLEE OOFF CCOONNTTEENNTTSS Introduction 1 Laboratory safety 4 Laboratory operations 8 Experiment 1: Esterification reaction: Synthesis of n-butyl acetate 17 Experiment 2: Esterification reaction: Preparation of aspirin 22 Experiment 3: Synthesis of benzoic acid and benzyl alcohol 27 Experiment 4: Nitration of phenol 33 Experiment 5: Synthesis of triphenylmethanol 37 Experiment

CHE 2401 Lab Manual 3 Getting along in the laboratory You will get along much better in the laboratory if you can maintain peace and harmony

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