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Lab Manual Synthesis and Reactions of Ferrocene Web

RCarbonRSynthesis and Reactions of FerroceneCarbonRCarbonContents Objectives 1 Introduction 1 Preparation of Ferrocene 2 Acetylation of Ferrocene 7 Preparation of [Fe( -C5H5)( -C6H6)]PF6 10 Reaction of [Fe( -C5H5)( -C6H6)] PF6 with nucleophiles 12 Manuscript prepared by Dr. Almas I. Zayya, Dr. A. Jonathan Singh and Prof.

provide experience in the synthesis, isolation, purification and characterisation of organometallic compounds. Purification techniques include distillation, sublimation, chromatography and crystallisation. The main characterisation technique used in these experiments is 1H NMR spectroscopy using the benchtop Spinsolve spectrometer.

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