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METHOD 8260B VOLATILE ORGANIC COMPOUNDS BY GAS ...

CD-ROM8260B - 1 Revision 2 December 1996 METHOD 8260 BVOLATILE ORGANIC COMPOUNDS BY GAS CHROMATOGRAPHY/MASS SPECTROMETRY (GC/MS) AND 8260 is used to determine VOLATILE ORGANIC COMPOUNDS in a variety of solid wastematrices. This METHOD is applicable to nearly all types of samples, regardless of water content,including various air sampling trapping media, ground and surface water, aqueous sludges, causticliquors, acid liquors, waste solvents, oily wastes, mousses, tars, fibrous wastes, polymericemulsions, filter cakes, spent carbons, spent catalysts, soils, and sediments. The followingcompounds can be determined by this METHOD :Appropriate Preparation Techniquea 5030/DirectCompoundCAS (Propenal)107-02-8ppccndndcAcrylonitrile 107-13-1ppccndccAllyl alcohol107-18-6htcndndndcAllyl chloride107-05-1cndndndndcBenzene71-43-2 cndccccBenzyl chloride100-44-7cndndndndcBis(2-chloroet hyl)sulfide505-60-2ppndndndndcBromoaceto ne598-31-2ppndndndndcBromochloromethane 74-97-5cndccccBromodichloromethane75-27- 4cndcccc4-Bromofluorobenzene (surr)460-00-4cndccccBromoform75-25-2cnd ccccBromomethane74-83-9cndccccn-Butanol7 1-36-3htcndndndc2-Butanone (MEK)78-9

(Method 3585) for waste oil samples; automated static headspace by Method 5021 for solid sa mples; direct injection of an aqueous sample (concentration permitting) or injection of a sample concentrated by azeotropic distillation (Method 5031); and closed system vacuum distillation (Method 5032) for aqueous, solid, oil and tissue samples.

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