Transcription of NMR Proton Shifts for Residual Solvent Impurities
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NMR Proton Shifts for Residual Solvent Impurities
SolventSynonymsMol Wt BP C Linear Formula H-Signal Multi CDCl3 D2O CD3OD (CD3)2SO(CD3)2 COCD3 CNC6D6 Acetic AcidEthanoic AcidMethanoic 1-Butanoln-Butanol / 1-Hydroxybutane / n-Butyl (CH2) CH2 (3) CH2 (2) CH2 (1) 2-Butanolsec-Butanol / 2-Butyl alcohol / 2-Hydroxybutane (OH)CH2CH3CH3 (4) CH3 (1) tert-Butanolt-Butyl alcohol / 2-Methyl-2-propanol (CH3) GlycolEthane-1,2-diol / 1,2-Dihydroxyethane / Hexyl alcohol / Caproic alcohol (CH2) CH2 (3-5) CH2 (2) CH2 (1) iso-Amyl alcohol3-Methyl-1-butanol / iso-Pentyl alcohol (CH3) iso-Butanoliso-Butyl alcohol / (CH3) MethanolMethyl alcohol / Pentyl alcohol (CH2) CH2 (3-4) CH2 (2) CH2 (1) 1-Propanoln-Propanol / Propyl alcohol CH2 (2) CH2 (1) 2-PropanolIPA / Isopropanol / iso-Propyl alcohol (CH3) / Methyl phenyl ether CH (o/p) CH (m) (2) (3) (4) (o/p) (m) 1,4-Dimethylbenzene / p-Xylol (CH3) ChloroformTrichloromethane / Formyl ,2-DichloroethaneEDC / Ethylene dichloride / Glycol dichloride / Methylene dichloride / Methyl cyanide / Cyanomethane / (CH3) sulfoxideDMSO / Methyl sulfoxide / (Methylsulfinyl) (CH3) acetate1-Butyl
Chloroform Trichloromethane / Formyl trichloride 119.38 61 CHCl 3 CH s 7.26 – 7.88 8.32 8.02 7.58 6.15 1,2-Dichloroethane EDC / Ethylene dichloride / Glycol dichloride 98.96 81-85 ClCH
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