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PRACTICAL LAB MANUAL

PRACTICAL LAB MANUAL . LAB MANUAL PHARMACEUTICAL ORGANIC CHEMISTRY-I. (B. Pharm Ist Year). CONTENTS. Chapters Pages Lassaigne`s extract (sodium fusion extract) and detection of 1. 1. elements 2 General pattern of functional group tests 4. 3. Functional group test: test for carboxylic acid 6. 4. Functional group test: test for alcohol 9. 5. Functional group test: test for phenols 12. 6. Functional group test: test for esters 16. Functional group test: test for carbonyl group- aldehyde and 7. ketone 17. Functional group test: test for primary, secondary and tertiary 8. amines 22. 9. Functional group test: test for anilides 26. 10. Functional group test: test for amides 27. 11. Functional group test: test for nitroso group 28. 12. Functional group test: test for carbohydrates 29. 13. Identification and reactions of hydrocarbons 30. 14. Derivative preparation 33. 15. Synthesis of aspirin 40.

26. Synthesis of hippuric acid 51 27. Synthesis of barbituric acid 52 28. Synthesis of 1,2,3,4-tetrahydrocarbazole 53 29. Synthesis of 7-hydroxy-4-methyl coumarin 54

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