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Quick Method for the LC-MS/MS Analysis of Highly …

EU Reference Laboratory for pesticides requiring Single Residue Methods (EURL-SRM) CVUA Stuttgart, Schaflandstr. 3/2, DE-70736 Fellbach, Germany Website: , E-Mail: 1 of 60 Quick Method for the Analysis of numerous Highly Polar Pesticides in Foods of Plant Origin via LC-MS/MS involving Simultaneous Extraction with Methanol (QuPPe- Method ) - Version (March 2015, Document History, see page 58) Authors: M. Anastassiades; D. I. Kolberg; E. Eichhorn; A. Benkenstein; S. Luka evi ; D. Mack; C. Wildgrube; I. Sigalov; D. D rk; A. Barth Content 1 Scope and Short Description 2 2 Apparatus and Consumables 2 3 Chemicals 4 4 Disclaimer 6 5 Procedure 7 Sample preparation 7 Extraction / Centrifugation / Filtration 7 Blank extracts 9 Recovery experiments 9 Preparation of calibration standards 9 LC-MS/MS Measurement 12 Practical Information: Methods currently routinely used at CVUA Stutt

EU Reference Laboratory for pesticides requiring Single Residue Methods (EURL-SRM) CVUA Stuttgart, Schaflandstr. 3/2, DE-70736 Fellbach, Germany

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