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Supporting Information - authors.library.caltech.edu

Supporting Information Wiley-VCH 201469451 Weinheim, GermanyEnantioselective Synthesis ofa-Secondary anda-Tertiary Piperazin-2-ones and Piperazines by Catalytic Asymmetric Allylic Alkylation**Katerina M. Korch, Christian Eidamshaus, Douglas C. Behenna, Sangkil Nam, David Horne,and Brian M. Stoltz* 1 Supporting Information Table of Contents: Materials and Methods Representative Procedure 1 for the Preparation of 3-Oxopiperazine-2-carboxylates and 1,4-Diazepane-2-carboxylates Representative Procedure 2 for the Preparation of 3-Oxopiperazine-2-carboxylates Procedure for the Preparation of Allyl 4-benzoyl-2-methyl-3-oxo-1-phenylpiperaz ine-2-carboxylate (8p) Procedure for the Preparation of Allyl 4-benzoyl-1,2-dimethyl-3-oxopiperazine-2 -carboxylate (8q)

Supporting Information for Stoltz, et al. SI2# Materials and Methods.Unless otherwise stated, reactions were performed in flame-dried glassware under an inert atmosphere of argon or nitrogen using dry, deoxygenated

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