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Temperature calibration of differential scanning …
Journal of thermal Analysis, Vol. 45 (1995) 1285-1296 1995 Akad miai Kiad , BudapestJohn Wiley & Sons, Limited ChicesterTEMPERATURE calibration OF DIFFERENTIALSCANNING CALORIMETERSD. M. PriceCourtaulds Research & Technology, PO Box 111, Lockhurst Lane, COVENTRY CV6 5RS, UK(Received November 30, 1994)AbstractA procedure for calibrating the Temperature scale of a DSC is described. A different calibration trend wasobtained using the transition points of organic compounds compared to that found using the melting points ofhighly pure metals. The crystal-crystal transitions of three ammonium salts were studied by this method;ammonium dihydrogen phosphate and ammonium sulphate were found to be suitable reference materials in theregion -150 to 0 C, but ammonium nitrate was found to be unsuitable due to poorly
PRICE: TEMPERATURE CALIBRATION J. Thermal Anal., 45, 1995 3 Results and discussion Transition temperatures were taken as the extrapolated onset temperature (T
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