Transcription of 过渡元素XPS分析II--数据处理
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过渡元素XPS分析II--数据处理
XPS II-- XPS analysis for transition-metal elements (II): Data processing XPS XPS Introduction to General rules for XPS analysis method, and XPS Vocabulary Shirley Tougaard Seah REELS XPS CK 3 1s22s22p63s23p63dn4s2 .. XPS * Ti2+ , 3+ , 4+ ; Fe2+,3+; Cr2+,3+,6+; Mn2+ , 3+ , 4+ ; V3+,4+,5+; Co2+,3+; Ni2+,3+ Cu1+,2+; Zn1+,2+ Sb2+,5+; Sn2+,4+ - XPS Shake-up HAS CAE (IERF) )()(EEjEj =j0(E) j(E) IERF ~ E = 0 ~ -1 E KE IERF=E-1 KE=500eV IERF= Avantage IERF= Emin J(E) Shirley Background =+maxminmaxmin1)()()()()(EEkEEkkdTTFdTTF EjEjEFk F1(E)=j(E)=j0(E) Fk+1(Emin)=0 Fk+1(Emax)=j(Emax)
B=295 、C=657、D=295 eV 2 0.00E+00 5.00E+03 1.00E+04 1.50E+04 2.00E+04 2.50E+04 160 150 140 130 120 110 100 90 80 70 Counts / s Binding Energy (eV) Al2p Al2s 0.00E+00 1.00E+04 2.00E+04 3.00E+04 160 150 140 130 120 110 100 90 80 70 Counts / s Binding Energy (eV) Al2p Al2s 等离激元峰可以通过Tougaard
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