TA INSTRUMENTS DIFFERENTIAL SCANNING CALORIMETER …
gloves or use forceps when handling your DSC sample. DSC samples should be small enough to fit in one of the aluminum DSC pans. Powder samples or flat solid samples (less than 2 mm tall) work best, although other sample geometries are allowed. Sample weight should be between 0.5 and 100 mg. DSC sample preparation procedures are as follows: 1.
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www.eng.uc.edu1) Samples of irregular form can topple over in the pan. 2) Polymer films that have not been pressed against the base of the pan first change shape (no longer lie flat) on initial warming. Afterward, on melting, they make good contact with the pan (Fig. 2). b)An abrupt change of the heat transfer between the pan and the DSC sensor: