23．原子吸光光度法 - pref.kagawa.lg.jp

1 2006 18 3 31 0331030 .. 1.. 2.. g .. KOH mg .. g . mL 95 100 . mL . 10 . mL . mL . a b N c d a mL . b mL . c . d g . N .. H2O I2 SO2 3C5H5N 2(C5H5N H)I C5H5N SO3. C5H5N SO3 CH3OH (C5H5N H)O SO2 OCH3.. 3.. 30 .. 10 30 .. 10 50mg .. 30 .. 4. a f H2O) 100. W. a mL . W mg . f mL H2O mg .. 20mL . 10 50mg . 30 .. (b f c f ' . H2O) 100. W. b mL . c mL . W mg . f mL H2O mg . f ' mL H2O mg .. mg .. 30 . C . A .. 5.. C. H2O) 100. W. C . W mg .. 102g . 900mL 30 . 64g 12g .. 1000mL . 2,2' 24g . 100mL .. 1,3 4 40g 30g 200mL 25g 50mL g . 500mL .. 30g 100mL.. 100g . : 900mL. 64g 20g . 25g . 1000mL .. 6.. 2870cm-1 2850cm-1 . 18 1589cm-1 1583cm-1 . 12 . cm-1 .. 3000 1000cm-1 . 3000cm-1 cm-1. 1000cm-1 cm-1 .. 80 .. 4000 400cm-1 .. 2000cm-1 10cm-1 2000cm-1 cm-1. A Bcm-1. Bcm-1 Acm-1 .. mg .. 7.. 10cm . m . ATR . ATR .. mg m .. 8.. 4000 400cm-1 .. 10 30 30 60 .. A . B .. C . D . E . F . G . H . I . J . 9.. N mg . A g . mL.

2 ML .. 20mL . E J 25 . 15mL . I F 30mL . 10mL G . 80 100mL .. mL N.. 48 . 10. 200mL mL .. 10 30 30 60 .. A 300mL . B . C . D . E . F . G .. N 20 30mg . A . 20mL .. 150mL .. F 25mL 50mL E . B 85mL . C . 11. / .. mL N.. d . dl . 3,4 .. N . N 20 .. 40 . N .. N .. N .. N .. g 90 .. JIS Q0030 . 12.. Zn JIS K8005 .. CH3CN K8032 .. HOSO2NH2 JIS K8005 .. H2SO3.. SO2 . 25mL 10mL . mL 1mL .. mL SO2. 13. (iso) . (iso) 2 .. 2 .. 2,2' C4H11NO2 HCl . 20. n D 20. d 20 g mg .. 2 2 .. 95 . 14. 95 C2H5OH K8102 .. C2H5OH K8101 .. CH2=C(CH3)COO(CH2)2N (CH3)2CH2CH3 CH3CH2SO4 .. pH 10g 100mL pH .. 100 .. 200 75 m . 120 10 500 .. CaCl2 K8125 .. 15. NaCl JIS K8005 .. LiCl .. 2 .. mol/L. mL 1000mL . mol/L . 2,2' .. 2 2 1000mL .. 16.. 20M .. 63g 100mL .. 500mL 24 .. 102g . 350mL 25 30 . 64g 50g 24 .. 220mL . 17. 32g 2 81g .. 180mL 36g 24 .. 25mL . 50mg . mL H2O mg f .. f H2O mg mL . f 20mL .. f f ' mL mL . f ' mL H2O mg .. 2 2 .. N 2 C10H17NO6.

3 18.. 2(Na2O) 6(Al2O3) 12(SiO2) 6(K2O) 6(Al2O3) 12(SiO2) . mm .. g 500 700m2 .. [(CH3)3 NCH2CH2OH]Cl . 303 305 . g mg .. 1000mL 30g . 16 . mL .. , . 19. , 2,2 . , . 1,3 4 C13H14N2 . 61 62 . g mg .. N,N .. N,N HCON(CH3)2 K8500 .. C2Na2O4 JIS K8005 .. Pb(NO3)2 K8563 .. 20.. mol/L. 70g 50mL 95 1000mL .. 21.. Na2CO3 10H2O K8624 .. Na2CO3 JIS K8005 .. C4H6O3 . 240 242 . g mg .. 1000mL 30g . 16 . mL .. N,N .. N,N . N,N 100mL .. 22. 2 .. 2 2 . d .. 1 C12H26O .. K2Cr2O7 JIS K8005 .. p .. CH3NO2 K9523 .. C15H26O . 23.. 2,2 C10H8N2 K8486 .. C6H4(COOK) (COOH) JIS K8005 .. NaF JIS K8005 .. n . n 1 . 24. n . 1 CH3(CH2)2OH K8838 . 2 (CH3)2 CHOH K8839 . 2 . 2 . 2 . 2 .. 2 .. C21H14Br4O5S K8840 . 25. pH .. 50mg 95 100mL .. 100mL .. 2 . 2 100mL.. 10g g .. K3Fe(CN)6 K8801 . K4Fe(CN)6 3H2O K8802 .. g 10mL .. 100mL . 26.. g 10mL .. mol/L. 100mL .. 1 C7H15 NaO3S .. g 20mL.. 20M .. C12H25 NaO4S (C2H4O)2 .. mL C12H25 NaO4S (C2H4O)2.

4 C15H30O2 95 . 27.. pH .. C22H42O2 .. 2 C11H22NO6P .. 2 C6H8N2 . 20. d 20 200 202 . g mg . 2 . 2 . mL mg .. KIO3 JIS K8005 .. 28.. C13H26O2 98 .. 100mL .. 500mL . 500mL .. 29. 1000mL . NaHPO4 12H2O K9019 . 12 . Na2 HPO4 K9020 .. 1000mL . NaH2PO4 2H2O K9009 .. 48 . mL 50mL 15 . 25g .. mL HOSO2NH2.. 48 . mL 50mL 15 . 25g . 30.. mL HOSO2NH2. 1/60mol/L .. 1/60mol/L 1/60mol/L .. 1000mL Br . 15g 1000mL .. 1000mL Pb(NO3)2 . 1000mL .. 1000mL . 10mL 40mL 60mL mL mol/L mL mol/L . mol/L .. mol/L mL Na2SO4. mol/L .. mol/L . 1000mL NaOH . 31. 24 . g 25mL .. mol/L mL HOSO2NH2. mol/L .. mol/L . 24 . 25mL .. mol/L mL HOSO2NH2.. mol/L . mL HOSO2NH2.. mol/L . mL HOSO2NH2.. mol/L 32.. mL HOSO2NH2.. 1/60mol/L . 1000mL K2Cr2O7 . 100 110 .. 1000mL . L .. L . L-Cysteine Hydrochloride 20. D g mol/L 100mL .. p-Aminophenol 2000 mL . mL .. p-Phenylenediamine 33. 1000 mL . mL .. p-Aminophenol Sulfate 100 mL . mL .. 95 .. 34.. 100.

5 N,N .. 1 2 .. 35.. g . 50 100mL 254nm 15 .. 36.. Acrylic Acid Alkyl Methacrylate Copolymer C10 C30 .. Diglyceryl Adipate Mixed Fatty Acid Ester 270 290.. Sodium Bisulfite . SO2 . 50mL . mL .. 37. mL .. mL SO2.. Isostearyl Alcohol . 2950cm-1 2920cm-1 1465cm-1 1380cm-1 1365cm-1 1060 1035cm-1 .. Isostearic Acid . 2960cm-1 2920cm-1 1715 1700cm-1 1465cm-1 1285cm-1 1245cm-1 960 . 925cm-1 .. 2-Octyldodecyl Isostearate 2 . C38H76O2 .. 38.. Ethanol 15 C2H6O .. 96 .. 96 . Ethanol(96). 96 . 15 C2H6O .. N,N .. Ethyl[(methacryloyloxy)ethyl]dimethylamm onium Ethyl Sulfate N,N-Dimethyl Acrylamide Polyethylene Glycol Dimethacrylate Copolymer / Polyethylene Glycol Mixture N,N N,N . PEG .. N,N . 1540 . 25 35 .. ATR 3460 3430cm-1 2940cm-1 1725cm-1 1615cm-1. 1210cm-1 . 39.. ATR 2880cm-1 1465cm-1 1105cm-1 945cm-1.. 20ppm .. ppm .. 10mL 3000 . 30 20mL . m .. 100mL 200mL . 100mL 20 L .. 60ppm .. 220nm . 150mm m .. 40 .. : 1000mL.

6 12 . N,N N,N. 100mL . 200mL . 100mL 20 L .. N,N N,N . 60ppm . 40.. 220nm . 150mm m .. 25 .. N,N . g .. 30mL . 25 2500 30 . 30mL .. 80 .. g g 100.. 2-Octyldodecyl Erucate 13 2 . 2 C42H82O2 .. Hydrolyzed Collagen Solution Bos taurus Linn var. domesticus Gmelin (Bovidae) Sus scrofa Linn var. domesticus Gray (Suidae) .. 41.. N .. mL N. A B. A g 105 . B . d . d . d-Camphor d . mL 100mL . L . d QT . QS . d C10H16O mg MS QT QS . MS d mg . 25 .. mm m . 20M 180 250 m . 10 . 160 .. d .. L d .. L . d .. 42. dl . dl . dl-Camphor dl . mL 100mL . L . dl QT . QS . dl C10H16O mg MS QT QS . MS dl mg . 25 .. mm m . 20M 180 250 m . 10 . 160 .. dl .. L dl .. L . dl .. pH .. 7-Isopropyl-1,4-Dimethyl-3-Sodiumsulfona te Azulene 200 mL mL . 43.. pH 100mL pH .. mL . mL 30mL . 50mL 20ppm .. ppm . 2 .. 2 . Tri-2-Octyldodecyl Citrate 2 C66H128O7 .. N 2 .. Glyceryl-N-(2-Methacryloyloxyethyl)Carba mate Stearylmethacrylate Copolymer N 2.

7 40000 . N .. 3400 3350cm-1 2920cm-1 1730cm-1 1540cm-1 1470cm-1 1270cm-1 1160cm-1. 1050cm-1 .. 44. 20ppm .. ppm . N 2 . 2 10mL . mL mL . 30 . 2 100mL mL 20mL . mL 20mL . 20 L . N 2 . N 2 . N 2 . 250ppm .. 210nm . 15cm m .. 40 . 2 .. N 2 .. 20 L . N 2 2000.. 20 L . N 2 .. 2 . 10mL mL . mL 30 .. 100mL . 100mL. 20 L . 45.. 500ppm .. 210nm . 15cm m .. 40 . 2 .. 23 .. 20 L . 5000 . 20 L .. g 125 . , . mL N.. Condensate of Glycerin with Behenate and Eicosanedioate .. 2920cm-1 1745cm-1 1470cm-1 1165cm-1 720cm-1 .. 70mL . 180 230 g 200mL . 25mL 25mL.. 46. g . 20ppm . g . ppm . g .. R R. O O. H2. O O C 18 O O. R R. O O. n R H.. Cholesterol . 3450 3390cm-1 2930cm-1 1465cm-1 1375cm-1 1055cm-1 .. mg mL mL .. Ceric Oxide 16mL 10g 250mL . 47. 100mL . 10mL 17 100 g 15 . 200mL 15mL .. mL CeO2.. Polyglyceryl Diisostearate .. Rf . g 10mL .. 2 .. 2 . Neopentyl Glycol Di(Ethyl Hexanoate).. 300 330 mol/L 20mL .. Hexaglyceryl Dioleate 48.

8 Rf . g 10mL .. Polyglyceryl Distearate .. Rf . g 10mL .. Dimethyl Stearyl Amine .. 2920cm-1 2760cm-1 1465cm-1 1040cm-1 . g 2 50mL . 2 . 2 mL . 49. 180 190 . A. S. A 2 mL . S g . g 10mL .. Di(Isostearyl/Phytosteryl) Dilinoleate .. 2930cm-1 1740cm-1 1465 cm-1 1380cm-1 1170cm-1 . mL .. g . 20 10g . 70 100 g .. 20ppm .. ppm . g .. COOR. COOR'. R,R' H . 50. H .. Sodium Stearyl Sulfate 10mL . 60 .. Di(2-Octyldodecyl) N-Stearoyl-L-Glutamate N L 2 .. N . N-Stearoyldihydrosphingosine . 51. C36H73NO3 . 2S,3R .. N C36H73NO3 .. 3400cm-1 3320cm-1 2920cm-1 1635cm-1 . 50mg 40 mL 65 . mL . 25mg 20mL . L .. 30m . m . 100 10 220 220 . 20 . 250 .. 30cm . 100. 100 115 .. 20ppm .. ppm . 50mg 20mL . 50mL 10 L . 100 14 . 10cm . 1 200 100 10 . Rf . 20mL . 52. 50mL mL . 10mL 20 L .. N .. N .. mL 10mL . mL 10mL . mL 10mL . 20 L N . N . 13% . mL 10mL. 10 L .. N .. 210nm . 25cm m . S L tert . N .. 25 .. 19 . N 14 .. 10 20 . mL 20mL.

9 ML . 10mL 10 L N . N . 25 35 . g . 53. 50mg 20mL . 50mL mL . mL 10mL . 20 L . N . N .. N C36H73NO3 . A . 2500. mg . A mL mg .. N 50mg . 20mL . 50mL mL mL mL . mL 10mL . 20 L . N .. N .. 20mL .. 210nm . 25cm m .. 40 .. N 14 .. 20 L . N 10.. 20 L . 54. N .. Sodium Cetostearyl Sulfate 10mL . 60 .. Decaglyceryl Decaisostearate .. Rf . g 10mL .. Polyglyceryl Decaoleate .. 55. Rf . g 10mL .. Decaglyceryl Decastearate . 2920cm-1 1740cm-1 1465cm-1 1180 1165cm-1 .. Rf .. g 10mL .. 165 180.. Diglyceryl Tetraisostearate .. Rf . g 10mL .. 56.. Pentaerythritol Tetraisostearate .. 2960cm-1 2930cm-1 1745cm-1 1465cm-1 1380cm-1 1160 1145cm-1 .. E . E. Natural Vitamin E.. 50mL mL . 20mL mL . 500 2,2 200 . mL 25mL . 10 . 520nm AT mL . A0 . AT A0. 14100. W. AT . A0 . W mg .. Starch Sodium Acrylate Copolymer 57. 10g 95 100mL 10. G 50mL .. m . d .. d . d- -Tocopherol . 200 100mL 20mL .. 10 25 . 10 . mL C27H46O2. d . mL mL 30.

10 100mL mL n . 100mL mL . L . d n d d . d d .. S . d 100. Sn S . S d . Sn d .. mm . 125 150 m .. 280 . 58.. n 25 .. Glyceryl Triisostearate . 2950cm-1 2920cm-1 1750 1735cm-1 1465cm-1 1165 1145cm-1 .. Trimethylolpropane Triisostearate . 2960cm-1 2920cm-1 1745cm-1 1740cm-1 1465cm-1 1380cm-1 1365cm-1 . 1155cm-1 .. Polyglyceryl Trioleate .. Rf . g 10mL .. 59.. Decaglyceryl Tristearate .. Rf . g 10mL .. Palm Kernel Oil Amide Propyl Dimethyl Glycine Solution g . 20mL mL . mol/L 10 mL .. Bisabolol 100 . L . 17 . g 100g . 60. 105 20 . Rf . 2 .. 2 . 2-Octyldodecyl Pivalate 2 . 2 C25H50O2 .. DL .. DL . Sodium DL Pyrrolidonecarboxylate Solution pH . 80 . DL .. Phytosterol .. 61.. Fumaric Acid 30mL . mL . 50mL . 20ppm . 50mL .. Placental Extract(3).. g .. Polyglyceryl Heptastearate .. Rf . g 10mL .. 62.. Polyglyceryl Pentaisostearate .. Rf . g 10mL .. Polyglyceryl Pentaoleate .. Rf . g 10mL .. Decaglyceryl Pentastearate.