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1 172toll free: 800-338-1754 phone: 401-294-9400 fax: 401-295-2330 The EPA 8000 Methods RCRA Appendix IXReference Materials for Monitoring organic Pollutants in Ground WaterThe 8000 series Methods are used for monitoring organic pollutants in ground water as pre-scribed in the Resource Conservation and Recovery Act (see 40 CFR 264). These Methods may be found in EPA publication SW-846, Test Methods for Evaluating Solid Scientific has prepared a series of reference standards for the 8000 series Methods , as well as the necessary surrogate, internal, and calibration standards. Each component in a reference standard is pre-analyzed, with most analytes being >99% pure, and the solvents are of the highest quality available. All solutions are gravimetrically prepared to a precision of A certificate showing the actual weight of each analyte is supplied with mixture. Standards which are suitable for testing analytes found in Appendix IX to Resource Conservation and Recovery Act (40 CFR 264) are noted with a superscript IX.

2 View and download the EPA 8000 Methods at Method Page Method 8010B 173 Method 8011 174 Method 8015C 175 Method 8020A 176 Method 8021B 177 Method 8030A 179 Method 8031 179 Method 8032A 179 Method 8033 179 Method 8041A 180 Method 8061A 182 Method 8070A 183 Method 8080A 184 Method 8081B 186 Method 8082A 188 Method 8091 189 Method 8095 190 Method 8100 191 EPA Method Page Method 8121 193 Method 8141B 194 Method 8150B 196 Method 8151A 196 Method 8240b 198 Method 8260B 200 Method 8270D 204 Method 8280B 213 Method 8290A 213 Method 8310 214 Method 8315A 215 Method 8318A 215 Method 8330A 216 Method 8332 217 Method 8410 217 Method 8430 218 Method 8440 218 EPA 8000 MethodsW: : 1300 855 315173e-mail: web: IXEPA Method 8010 BVolatile HalocarbonsMethod 8010B is used to determine vola-tile halogenated organic pollutants, using either purge and trap or direct injection, and an electrolytic conductivity (Hall detector) Method 8010B has been deleted from the current revision of SW-846 (Update III).

3 To read the complete method, log onto our website at StandardsCalibration Standards: HCM-801 HC-070 HC-491 Surrogate Standard: STM-401 Technical Note2-Chloroethyl vinyl ether is stable in solu-tion by itself, but breaks down in the pres-ence of other halocarbons. Therefore ULTRA packages this analyte as a single component solution. If you prepare a working standard that contains 2-chloro-ethyl vinyl ether mixed with other halocar-bons, be sure to monitor the stability of this also Method 601, page Method 8010B Halogenated Volatiles Mixture IX36 Analytesallyl chloridebromodichloromethanebromoformbro momethanecarbon tetrachloridechlorobenzenechloroethanech loroformchloromethanedibromochloromethan e1,2-dibromo-3-chloropropane1,2-dibromoe thanedibromomethane1,2-dichlorobenzene1, 3-dichlorobenzene1,4-dichlorobenzenetran s-1,4-dichloro-2-butenedichlorodifluorom ethane1,1-dichloroethane1,2-dichloroetha ne1,1-dichloroethenetrans-1,2-dichloroet hene1,2-dichloropropanecis-1,3-dichlorop ropenetrans-1,3-dichloropropenemethylene chloridemethyl iodide1,1,1,2-tetrachloroethane1,1,2,2-t etrachloroethanetetrachloroethene1,1,1-t richloroethane1,1,2-trichloroethanetrich loroethenetrichlorofluoromethane1,2.

4 3-trichloropropanevinyl chloride@ 100 g/mL in MethanolHCM-801 4 x 1 mL ** HCM-801-1 1 x 1 mL ** Recommended Method 8010B Chloroprene Solutionchloroprene (no xylenes)@ 100 g/mL in MethanolHC-491 4 x 1 mL ** HC-491-1 1 x 1 mL ** Recommended Method 8010B Internal & Surrogate Standard Mix3 Analytes4-bromochlorobenzenebromochlorom ethane4-bromofluorobenzene@ 1500 g/mL in MethanolSTM-401 4 x 1 mL ** STM-401-1 1 x 1 mL ** Recommended Method 8010B 2-Chloroethyl Vinyl Ether Standards2-chloroethyl vinyl ether@ 100 g/mL in MethanolHC-070 4 x 1 mL **HC-070-1 1 x 1 mL ** @ 5000 g/mL in MethanolEPA-1016 1 x 1 mL **VOC Gas Mixtures6 Analytesbromomethanechloroethanechlorome thanedichlorodifluoromethanetrichloroflu oromethanevinyl chloride@ 200 g/mL in MethanolDWM-584 4 x 1 mL **DWM-584-1 1 x 1 mL ** @ 2000 g/mL in MethanolDWM-544 4 x 1 mL ** DWM-544-1 1 x 1 mL ** IX Contains Appendix IX Compounds8010BW: : 1300 855 315174toll free: 800-338-1754 phone: 401-294-9400 fax: 401-295-2330 Appendix IXEPA Method 8011 Dibromoethane and DibromochloropropaneMethod 8011 is used to determine 1,2-dibromoethane and 1,2-dibromo-3-chloro-propane, using microextraction, and capil-lary column GC with an read the complete method, log onto our website at StandardsCalibration Standard: DWM-504N HCM-812 Recommended Method 8011 Mixtures IX2 Analytes1,2-dibromo-3-chloropropane1,2-d ibromoethane@ 200 g/mL in MethanolDWM-504N 4 x 1 mL **DWM-504N-1 1 x 1 mL ** @ 2000 g/mL in MethanolHCM-812 4 x 1 mL **HCM-812-1 1 x 1 mL ** IX Contains Appendix IX Compounds 8011 Custom StandardsDo you require a standard not cataloged by ULTRA?

5 We catalog over 5500 different standards, but if you can t find the specific standard you need, we will be happy to prepare it for you on a custom basis. Our custom organic and inorganic standards are a fast, economical way to address your unique fax us a copy of the form found on page 399, or log on to and use our convenient quotation request web page. You will receive a quote within 24 choices available:Gravimetric Validation: All standards are manufactured under ULTRA s ISO 9001 registered quality system. Each analyte is guaranteed to be within the tolerance limits of nominal for inorganic analytes and nominal for organic analytes. A Certificate of Analysis accompanies each custom Validation: The method employed is identical to that used for all ULTRA cataloged standards and involves extensive instrumental analysis. All quantitative customs are provided with a DATApak and Certificate of Order by calling your Distributor Today!

6 W: : 1300 855 315175e-mail: web: IXEPA Method 8015 CNon-Halogenated Organics Method 8015C is used to determine vola-tile nonhalogenated organics, using either purge and trap or direct injection, and a flame ionization detector (FID).To read the complete method, log onto our website at StandardsCalibration Standard: NVM-8015A NVM-8015 BInternal Standard: STM-580 Non-Halogenated Volatiles Mixture IX4 Analytesdiethyl etherethyl alcohol2-butanone (MEK)4-methyl-2-pentanone (MIBK)@ 2000 g/mL in MethanolNVM-8115 4 x 1 mL **NVM-8115-1 1 x 1 mL ** Non-Halogenated Volatiles Mixture IX12 Analytesacetonitrileacrylamide2-butanone (MEK)diethyl ether1,4-dioxaneethyl alcoholethyl methacrylateisobutyl alcoholmethacrylonitrilemethyl methacrylate4-methyl-2-pentanone (MIBK)propionitrile@ 100 g/mL in MethanolNVM-8015 4 x 1 mL ** NVM-8015-1 1 x 1 mL ** Recommended Method 8015C Calibration Standard18 Analytesacetoneacetonitrileallyl alcohol1-butanol (n-butyl alcohol)tert-butyl alcohol (2-methyl-2-propanol)diethyl ether1,4-dioxaneethanolethyl acetateethylene glycolisobutyl alcohol (2-methyl-1-propanol)isopropyl alcohol (2-propanol)methanol2-butanone (MEK)4-methyl-2-pentanone (MIBK)2-pentanone1-propanol (n-propyl alcohol)

7 Propionitrile@ 2000 g/mL in WaterNVM-8015A 4 x 1 mL **NVM-8015A-1 1 x 1 mL ** Recommended Method 8015C Calibration Standard4 AnalytesN-nitrosodi-n-butylamine2-picoli nepyridineo-toluidine@ 2000 g/mL in MethanolNVM-8015B 4 x 1 mL ** NVM-8015B-1 1 x 1 mL ** GRO Aromatic Calibration Mix5 Analytesn-hexane (C6)n-heptane (C7)n-octane (C8)n-nonane (C9)n-decane (C10)@ 2000 g/mL in MethanolSAK-100 4 x 1 mL ** SAK-100-1 1 x 1 mL ** Recommended Method 8015C Internal Standard Mixture3 Analytes2-chloroacrylonitrilehexafluoro- 2-propanolhexafluoro-2-methyl-2-propanol @ 2000 g/mL in WaterSTM-580 4 x 1 mL ** STM-580-1 1 x 1 mL ** DRO Mixture10 Analytesn-decane (C10)n-dodecane (C12)n-tetradecane (C14)n-hexadecane (C16)n-octadecane (C18)n-eicosane (C20)n-docosane (C22)n-tetracosane (C24)n-hexacosane (C26)n-octacosane (C28)@ 2000 g/mL in Methylene ChlorideUST-200 4 x 1 mL ** UST-200-1 1 x 1 mL ** IX Contains Appendix IX Compounds8015CW: : 1300 855 315176toll free: 800-338-1754 phone: 401-294-9400 fax: 401-295-2330 Appendix IXEPA Method 8020 AAromatic Volatiles Method 8020A is used to determine vola-tile aromatic organic compounds, using either purge and trap or direct injection, and a 8020A has been deleted from the current revision of SW-846 (Update III).

8 To read the complete method, log onto our website at StandardsCalibration Standard: AMM-802 Internal and Surrogate Standard: STM-510 See also Method 602, page Method 8020A Aromatic Volatiles Mixture IX11 Analytesbenzenechlorobenzene1,2-dichloro benzene1,3-dichlorobenzene1,4-dichlorobe nzeneethylbenzenestyrenetolueneo-xylenem -xylenep-xylene@ 100 g/mL in MethanolAMM-802 4 x 1 mL ** AMM-802-1 1 x 1 mL ** Recommended Method 8020A Internal and Surrogate Standard Mixture5 Analytes4-bromochlorobenzene4-bromofluor obenzene1,4-difluorobenzenefluorobenzene a,a,a-trifluorotoluene@ 1500 g/mL in MethanolSTM-510 4 x 1 mL ** STM-510-1 1 x 1 mL ** Surrogate Standard Mixture3 Analytes4-bromochlorobenzene1,4-difluoro benzenefluorobenzene@ 2000 g/mL in MethanolSTM-420 4 x 1 mL ** STM-420-1 1 x 1 mL ** Surrogate Standard Mixture2 Analytes4-bromofluorobenzenea,a,a-triflu orotoluene@ 2000 g/mL in MethanolSTM-410 4 x 1 mL ** STM-410-1 1 x 1 mL ** Aromatic Volatiles Mixture IX10 Analytesbenzenechlorobenzene1,2-dichloro benzene1,3-dichlorobenzene1.

9 4-dichlorobenzeneethylbenzenetolueneo-xy lenem-xylenep-xylene@ 2000 g/mL in MethanolAMM-812 4 x 1 mL ** AMM-812-1 1 x 1 mL ** PVOC Mixture7 Analytesbenzeneethylbenzenemethyl tert-butyl ether (MTBE)tolueneo-xylenem-xylenep-xylene@ 1000 g/mL in MethanolUST-141 4 x 1 mL ** UST-141-1 1 x 1 mL ** Methyl tert-Butyl Ether Solutionmethyl tert-butyl ether (MTBE)@ 2000 g/mL in MethanolSTS-440 4 x 1 mL ** STS-440-1 1 x 1 mL ** Internal and Surrogate Standarda,a,a-trifluorotoluene @ 200 g/mL in MethanolSTS-221 4 x 1 mL **STS-221-1 1 x 1 mL ** @ 2000 g/mL in MethanolSTS-220N 4 x 1 mL **STS-220N-1 1 x 1 mL ** IX Contains Appendix IX Compounds 8020AW: : 1300 855 315177e-mail: web: Method 8021 BHalogenated and Aromatic volatile OrganicsMethod 8021B is used to determine aro-matic and halogenated volatiles, using either purge and trap, headspace, vacuum distillation, or direct injection. Detection is carried out with a PID and ELCD in read the complete method, log onto our website at StandardsCalibration Standards: DWM-588 HCM-822A HC-070 HC-491 Surrogate Standard: STM-431 Internal Standard: STM-240 NTechnical Note2-Chloroethyl vinyl ether is stable in solu-tion by itself, but breaks down in the pres-ence of other halocarbons.

10 Therefore ULTRA packages this analyte as a single component solution. If you prepare a working standard that contains 2-chloro-ethyl vinyl ether mixed with other halocar-bons, be sure to monitor the stability of this Method 8021B KitKit - contains six ampules:1 x 1 mL of each of the following standardsVOC Mixture (DWM-588-1)Halogenated Volatiles Mix (HCM-822-1)Chloroethyl Vinyl Ether Soln. (HC-070-1)Chloroprene Solution (HC-491-1)Surrogate Standard Mix (STM-431-1)Internal Standard Mix (STM-240N-1)AMK-8021 Kit **benzenebromobenzenebromochloromethaneb romodichloromethanebromoformbromomethane n-butylbenzenesec-butylbenzenetert-butyl benzenecarbon tetrachloridechlorobenzenechloroethanech loroformchloromethane2-chlorotoluene4-ch lorotoluenedibromochloromethane1,2-dibro mo-3-chloropropane1,2-dibromoethanedibro momethane1,2-dichlorobenzene1,3-dichloro benzene1,4-dichlorobenzenedichlorodifluo romethane1,1-dichloroethane1,2-dichloroe thane1,1-dichloroethenecis-1,2-dichloroe thenetrans-1,2-dichloroethene1,2-dichlor opropane1,3-dichloropropane2,2-dichlorop ropane1,1-dichloropropenecis-1,3-dichlor opropenetrans-1,3-dichloropropeneethylbe nzenehexachlorobutadieneisopropylbenzene 4-isopropyltoluenemethylene chloridenaphthalenen-propylbenzenestyren e1,1,1,2-tetrachloroethane1,1,2,2-tetrac hloroethanetetrachloroethenetoluene1,2,3 -trichlorobenzene1,2,4-trichlorobenzene1 ,1,1-trichloroethane1,1,2-trichloroethan etrichloroethenetrichlorofluoromethane1, 2,3-trichloropropane1,2.