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Agilent 8453 UV-visible Spectroscopy Systems - Young In

Agilent 8453 UV-visible Spectroscopy Systems Specifications Common Features provide fast access to frequently Productivity performed activities Agilent 8453 UV-visible Spectroscopy The Agilent 8453 system with manual Systems are based on a PC-controlled Stored methods are including all nec- sampling is already a highly productive spectrophotometer and a range of essary parameters to start immediate- UV-visible Spectroscopy system . For software products, each with fea- ly measurements after loading. example, the setup of an automated tures that meet the needs of specific analysis is done in a single dialog box. user groups. Agilent 8453 UV-visible You can use automation to guide an Regulatory Compliance Spectroscopy Systems include: operator through a series of manual Agilent 8453 spectrophotometer The built-in features of the measurements, or combine it without Agilent Chemstation general pur- Agilent 8453 spectrophotometer com- changes with sampling accessories to pose software for UV-visible bine with Agilent ChemStation to make provide semi- or fully-automated anal

Specifications Agilent 8453 UV-visible Spectroscopy Systems Common Features Agilent 8453 UV-visible spectroscopy systems are based on a PC-controlled

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Transcription of Agilent 8453 UV-visible Spectroscopy Systems - Young In

1 Agilent 8453 UV-visible Spectroscopy Systems Specifications Common Features provide fast access to frequently Productivity performed activities Agilent 8453 UV-visible Spectroscopy The Agilent 8453 system with manual Systems are based on a PC-controlled Stored methods are including all nec- sampling is already a highly productive spectrophotometer and a range of essary parameters to start immediate- UV-visible Spectroscopy system . For software products, each with fea- ly measurements after loading. example, the setup of an automated tures that meet the needs of specific analysis is done in a single dialog box. user groups. Agilent 8453 UV-visible You can use automation to guide an Regulatory Compliance Spectroscopy Systems include: operator through a series of manual Agilent 8453 spectrophotometer The built-in features of the measurements, or combine it without Agilent Chemstation general pur- Agilent 8453 spectrophotometer com- changes with sampling accessories to pose software for UV-visible bine with Agilent ChemStation to make provide semi- or fully-automated analy- Spectroscopy * it easy to comply with all of today's sis.

2 Automation controls the following PC with 17-inch monitor regulatory requirements, including 21 sampling Systems : Windows XP CFR Part 11. sipper system HP DeskJet printer A validation program which covers Agilent or Gilson autosamplers 1-cm quartz cell and check-out requirements for design qualifica- multicell transport sample tion, installation qualification and operational qualification. Spectral Acquisition * Additional software products are The Agilent 8453 fulfils all re- available for advanced tasks, kinetic quirements of the European All measurements contain full spectra, measurements, thermal denaturation, Pharmacopoeia (EP) and United which allows: dissolution testing or compliance with States Pharmacopeia (USP).

3 To change parameters like wave- 21 CFR Part 11 (Security Pack). Built-in tools for performance veri- length, background correction or fication (EP and USP tests) and even data type without re- measuring Ease of Use software validation. OQ/PV standards kit which meets to change the data analysis mode Agilent 8453 Spectroscopy Systems the needs of both EP and USP for without remeasuring, for example, use symbolic graphics to: convenience and time saving. quantification instead of an equa- make the system intuitive Compliance services are available tion provide confirmation of the cur- for software and hardware with to use the spectral information for rent status at a glance documentation created individual- identification, peak/valley find, or to provide visual confirmation of lually for the target configuration.

4 Diagnose measurement problems actions Flexibility General purpose software in- Biochemical analysis software, cluding verification and diag- including kinetics and thermal The Agilent ChemStation software is nostics, for standard applications. denaturation. modular to provide the functionality Advanced software for more ca- Dissolution testing software (sup- required for different tasks. To meet pabilities in data evaluation, ports Agilent 8453 only) for single these requirements four additional method development and auto- and multibath dissolution testing. software modules are available. mation. Security pack for compliance with FDA 21 CFR Part 11 (advanced and dissolution testing software only). Agilent ChemStation for UV-visible Spectroscopy : General Purpose Software General Description Data Analysis Tasks Quantification A virtually unlimited number of The general purpose software for Fixed Wavelength(s) standards can be used for the Agilent ChemStation is the core soft- Data at up to six wavelengths can calibration.

5 The only limit is the ware with instrument control, data be extracted from the spectrum. memory of the computer. acquisition, and a mode for standard Different types of background Concentration of Standards can data evaluation capabilities. A sepa- corrections can be applied. be entered directly by the user or rate mode allows diagnostic and veri- calculated from the given weight, fication of HP 8452A and Agilent 8453 Spectrum/Peaks volume, and purity from the soft- spectrophotometers. Finds up to specified number of ware. peaks and/or valleys in spectrum. Four calibration curves are avail- The general purpose software is spe- The last measured spectrum is able: linear, forced zero, linear, cially designed for ease of use in annotated with peaks and valleys.

6 Second order, forced zero, and routine labs or for occasional users. It The found peaks of all spectra are second order. allows to use the following data displayed in a results window. Calibration diagnostics include a types: plot of the processed spectra, a absorbance Ratio/Equation plot of each data point and the fit- transmittance The Equation mode allows the user to ted calibration curve. first to fourth derivative enter an equation for the evaluation Calibration curve statistics are the of data. The variables which have standard deviation for each cali- An Execute Advanced Method mode been entered for the samples are: bration coefficient, the standard allows execution of any method that Up to six specified wavelength deviation of calibration, and the was developed using the advanced values, weight and volume correlation coefficient.

7 Software for Agilent ChemStation. Mathematical functions include +, , , /, log, ln, exp, sqr, sqrt Automation Results are displayed in a window Automation comprises an automation with the values at the specified wave- table which consists of: lengths and the equation results. The up to three standards (only for results are automatically corrected quantification). for the pathlength of the cell and the two controls dilution factor. a user-defined number of samples (only limited by sampling device). The automatically-generated result Verification and Diagnostics The diagnostics allows the user to: report can include statistics on the check the lamp intensities samples (average, standard deviation, The general purpose software check the lamp stability % RSD, minimum and maximum includes a Verification and Diagnostic check the dark current value).

8 Automation normally, but not mode to allow the user to verify and check the pump time for a sip- necessarily, involves automated sam- diagnose the correct operation of per/autosampler system with a ple introduction as well as measure- HP 8452A or Agilent 8453 spectropho- flow test ment and evaluation. tometers. It allows to perform the fol- lowing tests: Operating system and PC. spectrophotometer self test Interactive Spectral Requirements performance verification checks Processing such as photometric and wave- Agilent ChemStation software is com- Spectra may be interactively proc- length accuracy patible with Microsoft Windows 2000. essed by the user with the following wavelength reproducibility and Windows XP. An IBM-compatible functions: stray light PC with Pentium III processor (600.)

9 Absorbance transmittance noise MHz or faster recommended), 128 MB. scalar add and multiply baseline flatness RAM, CD-ROM drive and SVGA. spectral add and subtract drift (1 hour, optional) graphics is required to operate the calculation of derivatives performance verification, in- software properly. Instrument control interpolation of data points by a cluding all tests required by the is done through GPIB or LAN. spline algorithm European Pharmacopoeia and ( Agilent 8453 only). United States Pharmacopeia Agilent 8453 UV-visible Spectrophotometer General Description Firmware upgrade from PC for Diode-array Advantages easy participation in future de- The Agilent 8453 offers the latest in velopments, and Backed by almost two decades of diode-array technology.

10 Built-in GPIO interface for control experience in the development and of accessories. manufacture of diode-array spec- Compliance with all requirements trophotometers, the Agilent 8453 . of the European Pharmacopoeia gives you clear advantages. (EP) and United States Regulatory Compliance Fast spectral scanning for com- Pharmacopeia (USP). The Agilent 8453 supports compliance plete spectral information and Small footprint to save bench with GLP regulations. multiwavelength applications space. Serial number and firmware revi- such as user-defined equations. Prealigned deuterium and tung- sion held in non-volatile memory. Open sample area for convenient sten lamp light sources for trou- Own clock for time and date sample handling.


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