Environmental Proficiency Testing Standards Certified ...

1 Environmental Proficiency Testing Standards Certified quality Control Standards2018 Certificate #: AR-1571 Certificate AT-1690 Certificate #: AR-1693 Certificate #: AP-1693 ALL PT SAMPLES ARE PROVIDED IN DUPLICATEQ uality Control PT Data Management 3-4 Proficiency Testing Programs/QC Standards 5-40 NPW Organics Proficiency Testing & quality Control Samples 5-10 NPW Inorganics Proficiency Testing & quality Control Samples 11-14 NPW Microbiological Proficiency Testing & quality Control Samples 15-16 DMRQA-38 17-19 WS Organics Proficiency Testing & quality Control Samples 20-24 WS Inorganics Proficiency Testing & quality Control Samples 25-27 WS Microbiological Proficiency Testing & quality Control Samples 28-29 UST Proficiency Testing & quality Control Samples 30-31 Soil/Hazardous Waste Proficiency Testing & quality Control Samples 32-40PT Express 41 Custom PT/QC Materials 41 Custom Solution Request Form 42 DMRQA-38 Order Form 43 Order Form 44 How To Do Business With NSI 45 Index 46

2 Table of ContentsNSI Lab Solutions7212 ACC BlvdRaleigh, NC 27617 Toll: : : PT SAMPLES ARE PROVIDED IN DUPLICATEPT samples have to be right. Your laboratory s accreditation is at stake, so anything less than 100% confidence is just not good s why we bring over 25 years of multidisciplinary reference material manufacturing and certification experience into every step of our process. And that s why our analytical validation specifications are more stringent than the current NELAC start by certifying the purity of analyte source materials and then correcting sample assigned values for this Certified purity. This correction increases the certainty of the assigned value. We document the accuracy of each formulation and the homogeneity of each batch by instrumental analyses of each analyte in each of the samples taken from the production run.

3 No sample is ever released into a PT study unless the results of this analytical process meet our acceptance limits, limits more stringent by 30% than the current NELAC Standards . We close the PT study by documenting the stability of every analyte in every sample. This is your assurance that the sample was still right when your lab analyzed it. We are a TNI approved PT provider holding the following accreditations: ISO 34, ISO 17025, ISO 17043, and ISO Accurate. Certified Stable. Every Analyte. Every , this QA process is intensive, but it works. In the years since PT privatization: We have never issued a PT report to a customer or accrediting agency containing inaccurately entered, reported, or assigned values. We have never released a PT sample into a study with an inaccurate assigned s our track record, and we provide this performance at an exceptional value.

4 All NPW and WS quantitative PT samples are always supplied in duplicate for prices comparable to other industry providers single-sample Value with Zero #: AR-1571 Certificate AT-1690 Certificate #: AR-1693 Certificate #: AP-1693 ALL PT SAMPLES ARE PROVIDED IN DUPLICATE Simplified on-line data entry and modification screens. Drop-down screens for NELAC method and technology codes. Download your PT reports as .pdf files. Monitor, sort, and review your PT results over time by methods and analytes in each FOT. Electronically report results to accrediting authorities. Direct upload of PT results from your LIMS. Analyte statistical summaries for each DatalinkMuch More Than On-Line Data EntryHave PT reports sent to as many accrediting authorities as you need without being nickeled and dimed. We do not charge for multiple reports. Make PT planning easier by accessing preliminary results on-line within 24 hours of the study assured your reports will be delivered to your accrediting authority securely and on time.

5 We use only overnight express service to provide PT results to your accrediting authority. This provides traceability and proof your reports were delivered on time!PT ReportsAs Many As You Need! When You Need Them!NSI Lab Solutions7212 ACC BlvdRaleigh, NC 27617 Toll: : : PT SAMPLES ARE PROVIDED IN DUPLICATENPW VolatilesA mL concentrate in Methanol for use with Methods 601/602, 8010/8020, 624, 8240, and 8260. The sample design will satisfy PT requirements for any of the following analytes:NPW Organics Proficiency Testing Studies (Available: January, March, April, July, September, October)Our studies include all analytes required by the NELAC NPW fields of Testing . Provided in duplicate, each ampule produces at least one liter of sample (with the exception of VOC s).PEO-120 $ QC Known $ PCB in WaterA mL concentrate in Acetone for use with Methods 608/8080 ,1-Dichloroethane10-150 ug/L1,1-Dichloroethene10-150 ug/L1,1,1-Trichloroethane10-100 ug/L1,1,1,2-Tetrachloroethane15-150 ug/L1,1,2-Trichloroethane15-150 ug/L1,1,2,2-Tetrachloroethane15-150 ug/L1,2-Dibromo-3-chloropropane15-150 ug/L1,2-Dichlorobenzene10-120 ug/L1,2-Dichloroethane15-150 ug/L1,2-Dichloropropane10-150 ug/L1,2,3-Trichlorobenzene15-150 ug/L1,2,3-Trichloropropane15-150 ug/L1,2,4-Trichlorobenzene15-150 ug/L1,2,4-Trimethylbenzene10-120 ug/L1,3,5-Trimethylbenzene10-120 ug/L1,3-Dichlorobenzene10-120 ug/L1,4-Dichlorobenzene10-120 ug/L1.

6 4-Dioxane20-500 ug/L2-Butanone5-500 ug/L2-Chloroethyl vinyl ether5-500 ug/L2-Hexanone20-200 ug/L4-Methyl-2-pentanone20-200 ug/LAcetone20-200 ug/LAcetonitrile5-500 ug/LAcrolein5-500 ug/LAcrylonitrile5-500 ug/LBenzene10-120 ug/LBromodichloromethane10-100 ug/LBromoform10-100 ug/LBromomethane20-120 ug/LCarbon disulfide5-500 ug/LCarbon tetrachloride15-150 ug/LChlorobenzene10-120 ug/LChloroethane20-120 ug/LChloroform10-100 ug/LChloromethane20-120 ug/Lcis-1,2-Dichloroethene10-150 ug/Lcis-1,3-Dichloropropene10-120 ug/LDibromochloromethane10-100 ug/LDibromomethane10-120 ug/LDichlorodifluoromethane20-100 ug/LEthylbenzene10-120 ug/LEthylene dibromide10-120 ug/LMethyl acetate5-500 ug/LMethyl cyclohexane20-100 ug/LMethylene chloride10-120 ug/Lm+p-Xylene10-150 ug/LMTBE15-150 ug/LNaphthalene15-150 ug/Ln-Hexane10-150 ug/Lo-Xylene10-150 ug/LStyrene20-120 ug/LTetrachloroethene10-150 ug/LToluene10-120 ug/LTotal Xylenes20-300 ug/Ltrans-1,2-Dichloroethene10-120 ug/Ltrans-1,3-Dichloropropene10-120 ug/LTrichloroethene10-100 ug/LTrichlorofluoromethane20-120 ug/LVinyl acetate5-500 ug/LVinyl chloride20-120 ug/LArochlor ug/LArochlor ug/LArochlor ug/LArochlor ug/LArochlor ug/LPEO-020 $ QC Known $ ug/LArochlor ug/LArochlor ug/LArochlor #: AR-1571 Certificate AT-1690 Certificate #.

7 AR-1693 Certificate #: AP-1693 ALL PT SAMPLES ARE PROVIDED IN DUPLICATENPW Organics Proficiency Testing Studies (Available: January, March, April, July, September, October)NPW Base/NeutralsA 2 x mL concentrate set for use with Methods 625/8270. The sample design will satisfy PT requirements for any of the following analytes:NOTE: This sample is provided in a two-ampule set. The Benzidine and 3,3 -Dichlorobenzidine are segregated to assure stability throughout the PT $ QC Known $ ,1-Biphenyl 30-200 ug/L1,2,4,5-Tetrachlorobenzene 20-200 ug/L1,2,4-Trichlorobenzene 20-200 ug/L1,2-Dichlorobenzene 20-200 ug/L1,2-Diphenylhydrazine 30-200 ug/L1,3,5-Trinitrobenzene 20-200 ug/L1,3-Dichlorobenzene 20-200 ug/L1,3-Dinitrobenzene 20-200 ug/L1,4-Dichlorobenzene 20-200 ug/L1,4-Dioxane 20-200 ug/L1,4-Naphthoquinone 20-200 ug/L1-Chloronaphthalene 20-200 ug/L1-Methylnaphthalene 30-200 ug/L1-Naphthylamine 20-200 ug/L2,3-Dichloroaniline 20-200 ug/L2,4-Dinitrotoluene 20-200 ug/L2.

8 6-Dinitrotoluene 20-200 ug/L2-Acetylaminofluorene 20-200 ug/L2-Chloronaphthalene 20-200 ug/L2-Methylcholanthrene 10-200 ug/L2-Methylnaphthalene 20-200 ug/L2-Naphthylamine 20-200 ug/L2-Nitroaniline 10-200 ug/L2-Picoline 20-200 ug/L3,3-Dimethylbenzidine 20-200 ug/L3,3 -Dichlorobenzidine 50-200 ug/L3-Methylcholanthrene 20-200 ug/L3-Nitroaniline 30-200 ug/L4-Aminobiphenyl 20-200 ug/L4-Bromophenyl phenyl ether 20-200 ug/L4-Chloroaniline 10-200 ug/L4-Chlorophenyl phenyl ether 20-200 ug/L4-Nitroaniline 10-200 ug/L4-Nitroquineoline-1-oxide 20-200 ug/L5-Nitro-o-toluidine 20-200 ug/L7,12-Dimethylbenz(a)anthracene 20-200 ug/La,a-Dimethylphenylamine 20-200 ug/LAcenaphthene 10-200 ug/LAcenaphthylene 10-200 ug/LAcetophenone 20-200 ug/LAniline 30-200 ug/LAnthracene 10-200 ug/LAtrazine 30-200 ug/LBenzaldehyde 30-200 ug/LBenzidine 200-1000 ug/LBenzo(a)anthracene 10-200 ug/LBenzo(a)pyrene 10-200 ug/LBenzo(b)fluoranthene 20-200 ug/LBenzo(g,h,i)perylene 10-200 ug/LBenzo(k)fluoranthene 20-200 ug/LBenzyl alcohol 30-200 ug/LBenzyl butyl phthalate 50-200 ug/Lbis(2-Chloroethoxy)methane 20-200 ug/Lbis(2-Chloroethyl)ether 20-200 ug/L2,2 -Oxybis(1-Chloropropane)bis(2-Ethylhexyl )phthalate 20-200 ug/LCaprolactam 30-200 ug/LCarbazole 20-200 ug/LChlorobenzilate 20-200 ug/LChrysene 10-200 ug/LDi-n-butyl phthalate 40-200 ug/LDi-n-octyl phthalate 30-200 ug/LDiallate 20-200 ug/LDibenz(a,h)

9 Anthracene 20-200 ug/LDibenzofuran 30-200 ug/LDiethyl phthalate 50-200 ug/LDimethoate 20-200 ug/LDimethyl phthalate 50-200 ug/LDinoseb 20-200 ug/LDiphenyl ether 20-200 ug/LDisulfoton 20-200 ug/LEthyl methanesulfonate 30-200 ug/LFamphur 20-200 ug/LFluoranthene 30-200 ug/LFluorene 10-200 ug/LHexachlorobenzene 20-200 ug/LHexachlorobutadiene 50-200 ug/LHexachlorocyclopentadiene 50-200 ug/LHexachloroethane 50-200 ug/LHexachlorophene 20-200 ug/LHexachloropropene 20-200 ug/LIndeno(1,2,3-c,d)pyrene 30-200 ug/LIsodrin 20-200 ug/LIsophorone 20-200 ug/LIsosafrole 20-200 ug/LKepone 20-200 ug/Lm-Dinitrobenzene 10-200 ug/LMethapyrilene 20-200 ug/LMethyl methanesulfonate 10-200 ug/LMethyl parathion 20-200 ug/Ln-Decane 20-200 ug/LN-Nitroso-di-n-butylamine 20-200 ug/LN-Nitroso-di-n-propylamine 30-200 ug/LN-Nitrosodiethylamine 20-200 ug/LN-Nitrosodimethylamine 75-200 ug/LN-Nitrosodiphenylamine 30-200 ug/LN-Nitrosomethylethylamine 20-200 ug/LN-Nitrosomorpholine 20-200 ug/LN-Nitrosopiperidine 20-200 ug/LN-Nitrosopyrrolidine 20-200 ug/Ln-Octadecane 20-200 ug/LNaphthalene 20-200 ug/LNitrobenzene 20-200 ug/Lo,o.

10 O-Triethylphoshorothioate 20-200 ug/Lo-Dinitrobenzene 10-200 ug/Lo-Toluidine 20-200 ug/Lp-Dimethylaminoazobenzene 20-200 ug/Lp-Dinitrobenzene 10-200 ug/Lp-Phenylenediamine 20-200 ug/LParathion 20-200 ug/LPentachlorobenzene 20-200 ug/LPentachlorohexane 20-200 ug/LPentachloronitrobenzene 20-200 ug/LPhenacetin 20-200 ug/LPhenanthrene 10-200 ug/LPhorate 20-200 ug/LPronamide 20-200 ug/LPyrene 10-200 ug/LPyridine 10-200 ug/LSafrole 20-200 ug/LSulfotepp 20-200 ug/LThionazin 20-200 ug/LNSI Lab Solutions7212 ACC BlvdRaleigh, NC 27617 Toll: : : PT SAMPLES ARE PROVIDED IN DUPLICATENPW - AcidsA mL concentrate in Acetone for use with Methods 604/8040/8041 or 625/8270. The sample design will satisfy PT requirements for any of the following analytes:NPW - OP PesticidesA mL concentrate in Acetone for determination of:NPW - Organochlorine PesticidesA mL concentrate in Ethyl Acetate for use with Methods 608/8080/8081.