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HIGH TEMPERETURE COMPOSITE MATERIALS - UPILEX

HIGH TEMPERETURE . COMPOSITE MATERIALS . RTM Resin : PETI-330. PREPREG : PETI-365E PREPREG. MATERIALS for High Temp. COMPOSITE UBE BPDA Technology PETI-330. Operation temperature PETI-330 PMR-15. Operation temperature PMR-15 300 PETI-PREPREG. 300 PETI-PREPREG. 200 200. PETI-5 PETI-5. PEEK. PEEK. 100 100. Thermo- Thermo- (oC). (oC). plastic Epoxy Epoxy plastic Difficult Good Low Excellent Processability Mechanical properties UBE AEROSPACE MATERIALS 2. Resin for RTM. Breakthrough Resin Technology for High Temperature COMPOSITE Fabrication by RTM. Licensed From the NASA Under US Patent 6,359,107. PETI-330 is a new high temperature resin for Resin Transfer Molding Properties Viscosity : ~ Pa s (280 C).

UBE AEROSPACE MATERIALS www.upilex.jp 13 Prepreg for High Temp. Composite PETI-365E Prepreg Neat Resin Properties Density 1.33g/cc ASTM D792 Tg 357°C ASTM E1356

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Transcription of HIGH TEMPERETURE COMPOSITE MATERIALS - UPILEX

1 HIGH TEMPERETURE . COMPOSITE MATERIALS . RTM Resin : PETI-330. PREPREG : PETI-365E PREPREG. MATERIALS for High Temp. COMPOSITE UBE BPDA Technology PETI-330. Operation temperature PETI-330 PMR-15. Operation temperature PMR-15 300 PETI-PREPREG. 300 PETI-PREPREG. 200 200. PETI-5 PETI-5. PEEK. PEEK. 100 100. Thermo- Thermo- (oC). (oC). plastic Epoxy Epoxy plastic Difficult Good Low Excellent Processability Mechanical properties UBE AEROSPACE MATERIALS 2. Resin for RTM. Breakthrough Resin Technology for High Temperature COMPOSITE Fabrication by RTM. Licensed From the NASA Under US Patent 6,359,107. PETI-330 is a new high temperature resin for Resin Transfer Molding Properties Viscosity : ~ Pa s (280 C).

2 Tg (cured) : 333 C. UBE AEROSPACE MATERIALS 3. Resin for RTM. Characteristics Easy Processing Tg 626 F/330 C. Solvent Free Non Toxic Tough, Micro-crack resistant resin Thermo Oxidative Stability Dry Powder @ Room Temperature Easy handling 12 month Shelf-life UBE AEROSPACE MATERIALS 4. Resin for RTM. Melt Viscosity vs. Temperature Curve +05 800. 700. +04. 600. Visicosity / Pa s o o 536 F (280 C) Temp. +03. 500. Temp. / o F. +02 400. 300. +01. 200. Viscosity +00. 100. 0. 0 50 100 150 200 250 300. Time / min UBE AEROSPACE MATERIALS 5. Resin for RTM. Data +11 +03. o o E' Tg : 626 F(330 C). +10 +02. E', E'' / dyn/ cm 2. +09 E'' +01. Tan . +08 +00. +07 Tan +06 +05 0 200 400 600 800 1000.

3 Temp. / o F. UBE AEROSPACE MATERIALS 6. Resin for RTM. High Temperature Durability (Isothermal Aging) of T650-35/8HS Laminates 50. Open Hole Compression PETI-330/T650. BMI-5270/T650. 40. Strength / ksi 30. 20. 10. 0. 0 50 100 500 1000. Time @ 288 C in Air / Hr. UBE AEROSPACE MATERIALS 7. Resin for RTM. PETI-330 COMPOSITE Micro-crack resistant Neat Resin Elongation PETI-330 8 . PMR-15 1%. PETI-5 32%. UBE AEROSPACE MATERIALS 8. Resin for RTM. How to make COMPOSITE by RTM (TBD).. Vacuum UBE AEROSPACE MATERIALS 9. Resin for RTM. Package z 1kg - 9kg 1kg polyethylene bottles in cardboard box z 10kg and up 10kg moisture proof bag in paper drum UBE AEROSPACE MATERIALS 10. Prepreg for High Temp.

4 COMPOSITE PETI-365E Prepreg Features and benefits Polyimide resin matrix Tg 365 F. Tough, Micro-crack resistant resin Alcohol based prepreg system similar with PMR family Thermo Oxidative Stability UBE AEROSPACE MATERIALS 11. Prepreg for High Temp. COMPOSITE PETI-365E Prepreg Typical Properties Carbon fiber T800-12k plane woven (320g/m2). Resin content 38~42wt%. Volatile content 11~14wt%. Water, Alcohol Tg=365 C. UBE AEROSPACE MATERIALS 12. Prepreg for High Temp. COMPOSITE PETI-365E Prepreg Neat Resin Properties Density ASTM D792. Tg 357 C ASTM E1356. Tensile at 73 F(23 C). Strength 128 MPa ASTM D882. Modulus Elongation at break 13%. Water absorption at 73 F(23 C) ASTM D570 saturation Coefficient thermal expansion 51ppm/ C ASTM E233.

5 Weight loss 527 F(275 C),500hrs Weight loss 572 F(300 C),500hrs UBE AEROSPACE MATERIALS 13. Prepreg for High Temp. COMPOSITE PETI-365E Prepreg Typical COMPOSITE Properties 73 F(23 C) 550 F(288 C) Method SBS Strength 69 MPa - ASTM D2344. Flexural Strength 815 MPa 479 MPa ASTM D790. Flexural Modulus 62 GPa 62 GPa COMPOSITE : PETI-365E/T800 12K plane woven 300x300x4mm,[90/0]12lay-up,Fiver volume 59%. UBE AEROSPACE MATERIALS 14. Prepreg for High Temp. COMPOSITE PETI-365E Prepreg Autoclave Processing Parameters 400 700oF,1hrs 350. 300. 480 oF,3hrs temp.. 250 200 300 oF,2hrs 150. 140 oF,2hrs 100. 50 0. Vacuum -30mmHg -760mmHg time . Pressure UBE AEROSPACE MATERIALS 15. Prepreg for High Temp.

6 COMPOSITE PETI-365E Prepreg UD PREPREG Cloth PREPREG. 500mm x 50m Roll 1000mm 50m Roll Delivery Time : 3 months Transport Temperature : < 6 C. Storage Temperature : < -18 C. UBE AEROSPACE MATERIALS 16.

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