METHOD 8270C SEMIVOLATILE ORGANIC …

1 CD-ROM8270C - 1 Revision 3 December 1996 METHOD 8270 CSEMIVOLATILE ORGANIC COMPOUNDSBY GAS CHROMATOGRAPHY/MASS SPECTROMETRY (GC/MS) AND 8270 is used to determine the concentration of SEMIVOLATILE ORGANIC compoundsin extracts prepared from many types of solid waste matrices, soils, air sampling media and watersamples. Direct injection of a sample may be used in limited applications. The following compoundscan be determined by this METHOD :Appropriate Preparation Techniquesb 3540/CompoundsCAS No35103520354135503580aAcenaphthene83-32 -9 XXXXXA cenaphthene-d (IS)

2 XXXXX10 Acenaphthylene208-96-8 XXXXXA cetophenone 98-86-2 XNDNDNDX2-Acetylaminofluorene 53-96-3 XNDNDNDX1-Acetyl-2-thiourea 591-08-2 LRNDNDNDLRA ldrin 309-00-2 XXXXX2-Aminoanthraquinone 117-79-3 XNDNDNDXA minoazobenzene 60-09-3 XNDNDNDX4-Aminobiphenyl 92-67-1 XNDNDNDX3-Amino-9-ethylcarbazole 132-32-1 XXNDNDNDA nilazine 101-05-3 XNDNDNDXA niline 62-53-3 XXNDXXo-Anisidine 90-04-0 XNDNDNDX Anthracene 120-12-7 XXXXXA ramite 140-57-8HS(43)NDNDNDXA roclor 101612674-11-2 XXXXXA roclor 122111104-28-2 XXXXXA roclor 123211141-16-5 XXXXXA roclor 124253469-21-9 XXXXXA roclor 124812672-29-6 XXXXXA roclor 125411097-69-1 XXXXXA roclor 126011096-82-5 XXXXXA zinphos-methyl 86-50-0HS(62)NDNDNDXB arban 101-27-9 LRNDNDNDLRB enzidine 92-87-5 CPCPCPCPCPB enzoic acid 65-85-0 XXNDXXBenz(a)anthracene 56-55-3 XXXXXB enzo(b)fluoranthene 205-99-2 XXXXXB enzo(k)fluoranthene 207-08-9 XXXXXB enzo(g,h,i)perylene 191-24-2 XXXXXB enzo(a)

3 Pyrene 50-32-8 XXXXXCD-ROM8270C - 2 Revision 3 December 1996 Appropriate Preparation Techniquesb 3540/CompoundsCAS No35103520354135503580ap-Benzoquinone106 -51-4 OENDNDNDXB enzyl alcohol100-51-6 XXNDXX"-BHC319-84-6 XXXXX$-BHC319-85-7 XXXXX*-BHC319-86-8 XXXXX(-BHC (Lindane)58-89-9 XXXXXBis(2-chloroethoxy)methane111-91-1 XXXXXBis(2-chloroethyl) ether111-44-4 XXXXXBis(2-chloroisopropyl) ether108-60-1 XXXXXBis(2-ethylhexyl) phthalate117-81-7 XXXXX4-Bromophenyl phenyl ether101-55-3 XXXXXB romoxynil1689-84-5 XNDNDNDXB utyl benzyl phthalate85-68-7 XXXXXC aptafol2425-06-1HS(55)NDNDNDXC aptan133-06-2HS(40)NDNDNDXC arbaryl63-25-2 XNDNDNDXC arbofuran1563-66-2 XNDNDNDXC arbophenothion786-19-6 XNDNDNDXC hlordane (NOS)57-74-9 XXXXXC hlorfenvinphos470-90-6 XNDNDNDX4-Chloroaniline106-47-8 XNDNDNDXC hlorobenzilate510-15-6 XNDNDNDX5-Chloro-2-methylaniline95-79-4 XNDNDNDX4-Chloro-3-methylphenol59-50-7 XXXXX3-(Chloromethyl))

4 Pyridine hydrochloride6959-48-4 XNDNDNDX1-Chloronaphthalene90-13-1 XXXXX2-Chloronaphthalene91-58-7 XXXXX2-Chlorophenol95-57-8 XXXXX4-Chloro-1,2-phenylenediamine95-83- 0 XXNDNDND4-Chloro-1,3-phenylenediamine513 1-60-2 XXNDNDND4-Chlorophenyl phenyl ether7005-72-3 XXXXXC hrysene218-01-9 XXXXXC hrysene-d (IS)XXXXX12 Coumaphos56-72-4 XNDNDNDXp-Cresidine120-71-8 XNDNDNDXC rotoxyphos7700-17-6 XNDNDNDX2-Cyclohexyl-4,6-dinitro-phenol1 31-89-5 XNDNDNDLR4,4'-DDD72-54-8 XXXXX4,4'-DDE72-55-9 XXXXX4,4'-DDT50-29-3 XXXXXD emeton-O298-03-3HS(68)NDNDNDXD emeton-S126-75-0 XNDNDNDXD iallate (cis or trans) 2303-16-4 XNDNDNDXCD-ROM8270C - 3 Revision 3 December 1996 Appropriate Preparation Techniquesb 3540/CompoundsCAS No35103520354135503580a2,4-Diaminotoluen e95-80-7DC,0E(42)NDNDNDXD ibenz(a,j)

5 Acridine224-42-0 XNDNDNDXD ibenz(a,h)anthracene53-70-3 XXXXXD ibenzofuran132-64-9 XXNDXXD ibenzo(a,e)pyrene192-65-4 NDNDNDNDX1,2-Dibromo-3-chloropropane96-1 2-8 XXNDNDNDDi-n-butyl phthalate84-74-2 XXXXXD ichlone117-80-6 OENDNDNDX1,2-Dichlorobenzene95-50-1 XXXXX1,3-Dichlorobenzene541-73-1 XXXXX1,4-Dichlorobenzene106-46-7 XXXXX1,4-Dichlorobenzene-d (IS)XXXXX43,3'-Dichlorobenzidine91-94-1 XXXXX2,4-Dichlorophenol120-83-2 XXXXX2,6-Dichlorophenol87-65-0 XNDNDNDXD ichlorovos62-73-7 XNDNDNDXD icrotophos141-66-2 XNDNDNDXD ieldrin60-57-1 XXXXXD iethyl phthalate84-66-2 XXXXXD iethylstilbestrol56-53-1AW,0S(67)NDNDNDX D iethyl sulfate64-67-5 LRNDNDNDLRD ihydrosaffrole56312-13-1 NDNDNDNDNDD imethoate60-51-5HE,HS(31)NDNDNDX3,3'-Dim ethoxybenzidine119-90-4 XNDNDNDLRD imethylaminoazobenzene60-11-7 XNDNDNDX7,12-Dimethylbenz(a)- anthracene57-97-6CP(45)

6 NDNDNDCP3,3'-Dimethylbenzidine119-93-7 XNDNDNDX","-Dimethylphenethylamine122-09 -8 NDNDNDNDX2,4-Dimethylphenol105-67-9 XXXXXD imethyl phthalate131-11-3 XXXXX1,2-Dinitrobenzene528-29-0 XNDNDNDX1,3-Dinitrobenzene99-65-0 XNDNDNDX1,4-Dinitrobenzene100-25-4HE(14) NDNDNDX4,6-Dinitro-2-methylphenol534-52- 1 XXXXX2,4-Dinitrophenol51-28-5 XXXXX2,4-Dinitrotoluene121-14-2 XXXXX2,6-Dinitrotoluene606-20-2 XXXXXD inocap39300-45-3CP,HS(28)NDNDNDCPD inoseb88-85-7 XNDNDNDXD ioxathion78-34-2 NDNDNDNDNDD iphenylamine122-39-4 XXXXX5,5-Diphenylhydantoin57-41-0 XNDNDNDX1.

7 2-Diphenylhydrazine122-66-7 XXXXXCD-ROM8270C - 4 Revision 3 December 1996 Appropriate Preparation Techniquesb 3540/CompoundsCAS No35103520354135503580aDi-n-octyl phthalate117-84-0 XXXXXD isulfoton298-04-4 XNDNDNDXE ndosulfan I 959-98-8 XXXXXE ndosulfan II33213-65-9 XXXXXE ndosulfan sulfate1031-07-8 XXXXXE ndrin72-20-8 XXXXXE ndrin aldehyde7421-93-4 XXXXXE ndrin ketone53494-70-5 XXNDXXEPN2104-64-5 XNDNDNDXE thion563-12-2 XNDNDNDXE thyl carbamate51-79-6DC(28)NDNDNDXE thyl methanesulfonate62-50-0 XNDNDNDXF amphur52-85-7 XNDNDNDXF ensulfothion115-90-2 XNDNDNDXF enthion55-38-9 XNDNDNDXF luchloralin33245-39-5 XNDNDNDXF luoranthene206-44-0 XXXXXF luorene86-73-7 XXXXX2-Fluorobiphenyl (surr)321-60-8 XXXXX2-Fluorophenol (surr)367-12-4 XXXXXH eptachlor76-44-8 XXXXXH eptachlor epoxide1024-57-3 XXXXXH exachlorobenzene118-74-1 XXXXXH exachlorobutadiene87-68-3 XXXXXH exachlorocyclopentadiene77-47-4 XXXXXH exachloroethane67-72-1 XXXXXH exachlorophene70-30-4AW,CP(62)

8 NDNDNDCPH exachloropropene1888-71-7 XNDNDNDXH examethylphosphoramide680-31-9 XNDNDNDXH ydroquinone123-31-9 NDNDNDNDXI ndeno(1,2,3-cd)pyrene193-39-5 XXXXXI sodrin465-73-6 XNDNDNDXI sophorone78-59-1 XXXXXI sosafrole120-58-1DC(46)NDNDNDXK epone143-50-0 XNDNDNDXL eptophos21609-90-5 XNDNDNDXM alathion121-75-5HS(5)NDNDNDXM aleic anhydride108-31-6 HENDNDNDXM estranol72-33-3 XNDNDNDXM ethapyrilene91-80-5 XNDNDNDXM ethoxychlor72-43-5 XNDNDNDX3-Methylcholanthrene56-49-5 XNDNDNDX4,4'-Methylenebis (2-chloroaniline)101-14-4OE,OS(0)NDNDNDL RCD-ROM8270C - 5 Revision 3 December 1996 Appropriate Preparation Techniquesb 3540/CompoundsCAS No35103520354135503580a4,4'-Methylenebis (N,N-dimethylaniline)

9 101-61-1 XXNDNDNDM ethyl methanesulfonate66-27-3 XNDNDNDX2-Methylnaphthalene91-57-6 XXNDXXM ethyl parathion298-00-0 XNDNDNDX2-Methylphenol95-48-7 XNDNDNDX3-Methylphenol108-39-4 XNDNDNDX4-Methylphenol106-44-5 XNDNDNDXM evinphos7786-34-7 XNDNDNDXM exacarbate315-18-4HE,HS(68)NDNDNDXM irex2385-85-5 XNDNDNDXM onocrotophos6923-22-4 HENDNDNDXN aled300-76-5 XNDNDNDXN aphthalene91-20-3 XXXXXN aphthalene-d (IS)XXXXX81,4-Naphthoquinone130-15-4 XNDNDNDX1-Naphthylamine134-32-7OS(44)NDN DNDX2-Naphthylamine91-59-8 XNDNDNDXN icotine54-11-5DE(67)NDNDNDX5-Nitroacenap hthene602-87-9 XNDNDNDX2-Nitroaniline88-74-4 XXNDXX3-Nitroaniline99-09-2 XXNDXX4-Nitroaniline100-01-6 XXNDXX5-Nitro-o-anisidine99-59-2 XNDNDNDXN itrobenzene98-95-3 XXXXXN itrobenzene-d (surr)

10 XXXXX54-Nitrobiphenyl92-93-3 XNDNDNDXN itrofen1836-75-5 XNDNDNDX2-Nitrophenol88-75-5 XXXXX4-Nitrophenol100-02-7 XXXXX5-Nitro-o-toluidine99-55-8 XXNDNDXN itroquinoline-1-oxide56-57-5 XNDNDNDXN-Nitrosodi-n-butylamine924-16-3 XNDNDNDXN-Nitrosodiethylamine55-18-5 XNDNDNDXN-Nitrosodimethylamine62-75-9 XXXXXN-Nitrosomethylethylamine10595-95-6 XNDNDNDXN-Nitrosodiphenylamine86-30-6 XXXXXN-Nitrosodi-n-propylamine621-64-7 XXXXXN-Nitrosomorpholine59-89-2 NDNDNDNDXN-Nitrosopiperidine100-75-4 XNDNDNDXN-Nitrosopyrrolidine930-55-2 XNDNDNDXO ctamethyl pyrophosphoramide152-16-9 LRNDND