Transcription of Solvent Retention Data
1 DB-624 - AlphabeticalColumn:DB-62430 m x mm , 3 mP/N:125-1334 Oven:40 C for 5 min40-260 C at 10 /min260 C for 3 minCarrier:Helium at 30 cm/sec (40 C)Injector:Split 1:10, 250 CDetector:FID, 300 CRetention (acetaldehyde diethyl acetal) acetic acrylic
2 Ethyl , , , ,3-butanedione (diacetal) (MEK) (crotyl alcohol) (butyl cellosolve) ethyl methyl (allyl chloride) , ,2-dibromo-3-chloropropane (DBCP) ,2-dibromoethane (EDB) , , , , , ,2-dichloroethane (ethylene dichloride) ,1-dichloroethylene (vinylidine chloride) , , , , , , , , , glycol monobutyl glycol monoethyl glycol monomethyl (diethylene glycol dimethyl ether) , , ,4-dimethyl-3-pentanone (diisopropyl ketone) ,6-dimethyl-4-heptanone (diisobutyl ketone) , , (dimethylformamide) (methyl sulfoxide) (cellosolve) glycolSolvent Retention DataSorted alphabetically and by Retention timeDB-624, DB-1, DB-WAX columns specified in USPM ethod 467 data SheetDB-624 - AlphabeticalColumn:DB-62430 m x mm , 3 mP/N:125-1334 Oven:40 C for 5 min40-260 C at 10 /min260 C for 3 minCarrier:Helium at 30 cm/sec (40 C)Injector:Split 1:10, 250 CDetector.
3 FID, 300 CRetention TimeCompoundRetention TimeCompoundAuthorDean RoodAgilent Technologies, Blue Ravine RoadFolsom, CA 95630 USA2 Retention TimeCompoundRetention TimeCompoundRetention glycol monobutyl glycol monoethyl glycol monomethyl vinyl (Freon 11) (propylene glycol dimethyl ether) , , , (cumene) (methyl cellosolve) (active amyl alcohol) (tert-amyl alcohol) (iso-amyl alcohol) (MIBK; methyl isobutyl ketone) tert-butyl ether (MTBE) , , (valeraldehyde) , , (ethyl vinyl ketone) (methyl vinyl ketone) (benzyl acetone) , (allyl alcohol) glycol (1,2-propanediol) (propargyl alcohol) methyl ethyl ,2,4, ,1,1, ,1,2, (tetrahydrofuran) ,2, ,2, ,3, ,1, ,1, ,2, ,1,2-trichlorotrifluoroethane (Freon 113) (triethylene glycol dimethyl ether) ,2,3-trimethylbenzene (hemimellitene) ,2,4-trimethylbenzene (pseudocumene)
4 ,3,5-trimethylbenzene (mesitylene) - RetentionColumn:DB-62430 m x mm , 3 mP/N:125-1334 Oven:40 C for 5 min40-260 C at 10 /min260 C for 3 minCarrier:Helium at 30 cm/sec (40 C)Injector:Split 1:10, 250 CDetector:FID, 300 CRetention (Freon 11) vinyl ,1-dichloroethylene (vinylidine chloride) ,1,2-trichlorotrifluoroethane (Freon 113) (allyl chloride) tert-butyl ether (MTBE) trans-1, , (allyl alcohol) acetate ethyl ethyl 3-penten-2-one (methyl vinyl ketone) ,3-butanedione (diacetal) methyl , , (MEK) , (propargyl alcohol) (tetrahydrofuran) ,1, , glycol monomethyl (propylene glycol dimethyl ether) (methyl cellosolve) , (tert-amyl alcohol)
5 Methyl ethyl ,2-dichloroethane (ethylene dichloride) (crotyl alcohol) (diethylene glycol dimethyl ether) (ethyl vinyl ketone) , (valeraldehyde) , , (acetaldehyde diethyl acetal) glycol monoethyl (cellosolve) , MIBK; methyl isobutyl ketone) (iso-amyl alcohol) (active amyl alcohol) , ,1, , ,4-dimethyl-3-pentanone (diisopropyl ketone) , glycol (1,2-propanediol) ,2-dibromoethane (EDB) (dimethylformamide) , ,1,1, acetateRetention TimeCompoundRetention TimeCompoundDB-624 - RetentionColumn:DB-62430 m x mm , 3 mP/N:125-1334 Oven:40 C for 5 min40-260 C at 10 /min260 C for 3 minCarrier:Helium at 30 cm/sec (40 C)Injector:Split 1:10, 250 CDetector.
6 FID, 300 (methyl sulfoxide) glycol monobutyl (cumene) (butyl cellosolve) , ,1,2, , ,2, glycol monomethyl ,3,5-trimethylbenzene (mesitylene) ,6-dimethyl-4-heptanone (diisobutyl ketone) ,2,4-trimethylbenzene (pseudocumene) , , glycol monoethyl ,2,3-trimethylbenzene (hemimellitene) , , , -methylphenyl ,2-dibromo-3-chloropropane (DBCP) , ,3, , , ,2, glycol monobutyl , (triethylene glycol dimethyl ether) ,2, -ethylphenethyl (benzyl acetone) , -ethylphenethyl ,2,4, , , , benzyl ether4 Retention TimeCompoundRetention TimeCompound5DB-1 - AlphabeticalColumn:DB-130 m x mm , 3 mP/N:125-1034 Oven:40 C for 5 min40-260 C at 10 /minCarrier:Helium at 30 cm/sec (40 C)Injector:Split 1:10, 250 CDetector:FID, 300 CRetention (acetaldehyde diethyl acetal) ethyl , , , ,3-butanedione (diacetal) (MEK.)
7 Methyl ethyl ketone) (crotyl alcohol) (butyl cellosolve) ethyl methyl (allyl chloride) ,4-dimethyl-3-pentanone (diisopropyl ketone) ,6-dimethyl-4-heptanone (diisobutyl ketone) , ,2-dibromo-3-chloropropane (DBCP) ,2-dibromoethane (EDB) , , , , , ,2-dichloroethane (ethylene dichloride) ,1-dichloroethylene (vinylidine chloride) , , , , , , , , , glycol monobutyl monoethyl monomethyl (diethylene glycol dimethyl ether) , , (dimethylformamide) (methylsulfoxide) , , (cellosolve) glycol monobutyl glycol monoethyl glycol monomethyl -ethylphenethyl -ethylphenethyl vinyl (Freon 11) (propylene glycol dimethyl ether) , , , (cumene) (methyl cellosolve) benzoateRetention TimeCompoundRetention TimeCompoundDB-1 - AlphabeticalColumn:DB-130 m x mm , 3 mP/N:125-1034 Oven:40 C for 5 min40-260 C at 10 /minCarrier:Helium at 30 cm/sec (40 C)Injector:Split 1:10, 250 CDetector:FID, 300 (active amyl alcohol) (tert-amyl alcohol) (iso-amyl alcohol) (MIBK.
8 Methyl isobutyl ketone) -methylphenyl tert-butyl ether (MTBE) , , (valeraldehyde) , , (ethyl vinyl ketone) (methyl vinyl ketone) (benzyl acetone) , (allyl alcohol) (propargyl alcohol) glycol (1,2-propanediol) methyl ethyl ,2,4, ,1,1, ,1,2, (tetrahydrofuran) ,2, ,2, ,3, ,1, ,1, ,2, ,1,2-trichlorotrifluoroethane (Freon 113) (triethylene glycol dimethyl ether) ,2,3-trimethylbenzene (hemimellitene) ,2,4-trimethylbenzene (pseudocumene) ,3,5-trimethylbenzene (mesitylene) TimeCompoundRetention TimeCompoundRetention (Freon 11) vinyl ,1-dichloroethylene (vinylidine chloride) (allyl chloride) (allyl alcohol) , ,1,2-trichlorotrifluoroethane (Freon 113) (propargyl alcohol) , tert-butyl ether (MTBE) (methyl vinyl ketone) ,3-butanedione (diacetal) (MEK.
9 Methyl ethyl ketone) , ethyl , , glycol methyl (methyl cellosolve) (tetrahydrofuran) ethyl methyl (tert-amyl alcohol) ,2-dichloroethane (ethylene dichloride) ,1, (propylene glycol dimethyl ether) , (crotyl alcohol) (ethyl vinyl ketone) , , methyl (diethylene glycol dimethyl ether) (valeraldehyde) , , ethyl glycol ethyl (cellosolve) glycol (1,2-propanediol) , (iso-amyl alcohol) , (acetaldehyde diethyl acetal) (MIBK; methyl isobutyl ketone) (active amyl alcohol) , (dimethylformamide) ,1, , , ,4-dimethyl-3-pentanone (diisopropyl ketone) (methyl sulfoxide) ,2-dibromoethane (EDB) , ,1,1, TimeCompoundRetention TimeCompoundDB-1 - RetentionColumn:DB-130 m x mm , 3 mP/N:125-1034 Oven:40 C for 5 min40-260 C at 10 /minCarrier:Helium at 30 cm/sec (40 C)Injector:Split 1:10, 250 CDetector.
10 FID, 300 ,1,2, glycol butyl (butyl cellosolve) ,2, , , glycol methyl (cumene) ,6-dimethyl-4-heptanone (diisobutyl ketone) ,3,5-trimethylbenzene (mesitylene) glycol ethyl ,2,4-trimethylbenzene (pseudocumene) , , , ,2,3-trimethylb
