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Basic- NMR- Experiments

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150Basic-NMR-ExperimentsMMO January 2000Version 2 - DETERMINATION OF THE PULSE-DURATION9SUMMARY9Experiment - Determination of the 90 1H Transmitter Pulse Duration9Experiment - Determination of the 90 13C Transmitter Pulse Duration10Experiment - Determination of the 90 1H Decoupler Pulse Duration10Experiment - The 90 1H Pulse with Inverse Spectrometer Configuration11Experiment - The 90 13C Decoupler Pulse with Inverse Configuration11Experiment - Composite Pulses12Experiment - Radiation Damping13Experiment - Pulse and Receiver Phases13Experiment - Determination of Radiofrequency Power14CHAPTER 3 - ROUTINE NMR SPECTROSCOPY AND STANDARD TESTS15SUMMARY15Experiment - The Standard 1H NMR Experiment15Experiment - The Standard 13C NMR Experiment16Experiment - The Application of Window Functions16Experiment - Computer-aided Spectral Analysis17Experiment - Line-Shape Test for 1H NMR Spectroscopy17Experiment - Resolution Test for 1H NMR Spectroscopy18Experiment - Sensitivity Test for 1H NMR Spectroscopy18Experiment - Line-Shape Test for 13C NMR Spectroscopy19Experiment - ASTM Sensitivity Test fo

Experiment 8.9 - Isotope Effects on Chemical Shielding 64 Experiment 8.10 - pK a Determination with 13C NMR 64 Experiment 8.11 - The Relaxation Reagent Cr(acac) 3 65 Experiment 8.12 - Determination of Paramagnetic Susceptibility by NMR 65 Experiment 8.13 - 1H and 13C NMR of Paramagnetic Compounds 66 Experiment 8.14 - The CIDNP Effect 67

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