Transcription of 2.2.46. CHROMATOGRAPHIC SEPARATION TECHNIQUES …
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2.2.46. CHROMATOGRAPHIC SEPARATION TECHNIQUES …
Supercritical fluid chromatographyEUROPEAN PHARMACOPOEIA solutions. In addition to theTOC water control,prepare suitable blank solutions or other solutions neededfor establishing the baseline or for calibration adjustmentsfollowing the manufacturer s instructions; run the suitability. Run the following solutions and recordthe responses:TOC water(rw);standard solution(rs);systemsuitability solution(rss). Calculate the percentage responseefficiency using the expression:Thesystemissuitableiftherespo nseefficiencyisnotlessthan85 per cent and not more than 115 per cent of the (ru).
EUROPEAN PHARMACOPOEIA 7.0 2.2.46. Chromatographic separation techniques Figure 2.2.46.-1. The peak may be defined by the peak area, or the peak height (h) and the peak width at half-height (wh), or the peakheight (h) and the peak width between the points of inflection(wi).In Gaussian peaks (Figure 2.2.46.-1) there is the following
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