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A Technical Guide for Static Headspace Analysis ... - …

Inside:Basic Principles of HeadspaceAnalysisInstrumentationSystem Optimization(Troubleshooting) Headspace ApplicationsRecommended Headspace AnalysisProductsTechnical GuideA Technical Guidefor Static HeadspaceAnalysis Using e of Cont entsInt roduction .. 2 Basic Principles of HeadspaceAnalysis .. 3 Partition Coefficient Phase Ratio Combining K and Derivatization/ReactionHeadspace Headspace Sample SizeInstrumentation .. 6 Gas-Tight Syringe Injection Balanced-Pressure System Pressure-Loop SystemSystem Optimization(Troubleshooting) .. 8 Sample Preparation Sample Via l Sample Vial Heater and Mixer Sampling Transfer Line Injection Port Interfac eHeadspace Applications .. 11 Blood Alcohol Analysis USP <467> European Pharmacopoeia TestsRecommended Headspace AnalysisProducts .. 15 Capillary Columns Guard Columns Press-Tight Connectors Analytical Reference Materials GC Accessoriestatic Headspace gas chromatography (GC) is a technique used for the concentra-tion and Analysis of vol atile organic compounds.

5 www.restek.com Compound of Interest Derivatizing Reagent Resulting Derivative fatty acids methanol esterification with boron trifluoride glycerol acetic anhydride

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