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Appendix K: Guidelines for Dietary Supplements …

2012 AOAC INTERNATIONALThis Appendix contains three complementary documents for the validation of Dietary Supplements and botanical methods:Part I: AOAC Guidelines for Single-Laboratory Validation of Chemical Methods for Dietary Supplements and BotanicalsPart II: AOAC Guidelines for Validation of Botanical Identifi cation MethodsPart III: Probability of Identifi cation: A Statistical Model for the Validation of Qualitative Botanical Identifi cation MethodsPART IAOAC Guidelines for Single-Laboratory Validationof Chemical Methods for Dietary Supplementsand BotanicalsContents 1 Defi Method of Performance Characteristics of a Method of Analysis 2 Single-Laboratory Validation Preparation of the Laboratory Identifi Method of Analysis or Reference Ruggedness Specifi c Variablesa. Analyte Additionb. Reextraction of the Extracted Residuec.

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