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ARTICULATES NOT OTHERWISE REGULATED, RESPIRABLEP …

NIOSH Manual of Analytical Methods (NMAM), Fourth Edition PARTICULATES NOT OTHERWISE REGULATED, RESPIRABLE 0600 DEFINITION: aerosol collected by sampler with 4- m median cut point CAS: None RTECS: NoneMETHOD: 0600, Issue 3 EVALUATION: FULLI ssue 1: 15 February 1984 Issue 3: 15 January 1998 OSHA: 5 mg/m NIOSH: no RELACGIH: 3 mg/m PROPERTIES: contains no asbestos and quartz less than 1%; penetrates non-ciliated portions of respira-tory systemSYNONYMS: nuisance dusts; particulates not OTHERWISE classifiedSAMPLINGSAMPLER: CYCLONE + FILTER (10-mm nylon cyclone, Higgins-Dewell [HD] cyclone, or aluminum cyclone + tared 5- m PVC membrane)FLOW RATE: nylon cyclone: L/min HD cyclone: L/min Al cyclone: L/minVOL-MIN: 20 L @ 5 mg/m -MAX: 400 LSHIPMENT: routineSAMPLESTABILITY: stableBLANKS: 2 to 10 field blanks per setACCURACYRANGE STUDIED: to 10 mg/m (lab and field)BIAS: dependent on dust size distribution [1]OVERALL precision (): dependent on size distribution [1,2]ACCURACY: dependent on size distribution [1]MEASUREMENTTECHNIQUE: GRAVIMETRIC (FILTER WEIGHT)ANALYTE: mass of respirable dust fractionBALANCE: mg sensitivity; use same balance before and after sample collectionCALIBRATION: National Instit

2. Precision: The figure 0.068 mg quoted above for the precision is based on a study [3] of weighing procedures employed in the past by the Mine Safety and Health Administration (MSHA) in which filters are pre-weighed by the filter manufacturer and post-weighed by …

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