Transcription of Basic- NMR- Experiments
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Basic- NMR- Experiments
150 Basic- NMR-ExperimentsMMO January 2000 Version 2 - DETERMINATION OF THE PULSE-DURATION9 SUMMARY9 Experiment - Determination of the 90 1H Transmitter Pulse Duration9 Experiment - Determination of the 90 13C Transmitter Pulse Duration10 Experiment - Determination of the 90 1H Decoupler Pulse Duration10 Experiment - The 90 1H Pulse with Inverse Spectrometer Configuration11 Experiment - The 90 13C Decoupler Pulse with Inverse Configuration11 Experiment - Composite Pulses12 Experiment - Radiation Damping13 Experiment - Pulse and Receiver Phases13 Experiment - Determination of Radiofrequency Power14 CHAPTER 3 - ROUTINE NMR SPECTROSCOPY AND STANDARD TESTS15 SUMMARY15 Experiment - The Standard 1H NMR Experiment15 Experiment - The Standard 13C NMR Experiment16 Experiment - The Application of Window Functions16 Experiment - Computer-aided Spectral Analysis17 Experiment - Line-Shape Test for 1H NMR Spectroscopy17 Experiment - Resolution Test for 1H NMR Spectroscopy18 Experiment - Sensitivity Test for 1H NMR Spectroscopy18 Experiment - Line-Shape Test for 13C NMR Spectroscopy19 Experiment - ASTM Sensitivity Test for 13C NMR Spectroscopy20 Experiment - Sensitivity Test for 13C NMR Spectroscopy20 Experiment - Quadrature Image Test21 Experiment - Dynamic Range Test
Experiment 4.13 - 1H Single Frequency Decoupling of 13C NMR Spectra 30 Experiment 4.14 - 1H Low Power Decoupling of 13C NMR Spectra 31 Experiment 4.15 - Measurement of the Heteronuclear Overhauser Effect 32 CHAPTER 5 - DYNAMIC NMR SPECTROSCOPY 33 SUMMARY 33 Experiment 5.1 - Low Temperature Calibration with Methanol 33
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