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Basic- NMR- Experiments

150 Basic- NMR-ExperimentsMMO January 2000 Version 2 - DETERMINATION OF THE PULSE-DURATION9 SUMMARY9 Experiment - Determination of the 90 1H Transmitter Pulse Duration9 Experiment - Determination of the 90 13C Transmitter Pulse Duration10 Experiment - Determination of the 90 1H Decoupler Pulse Duration10 Experiment - The 90 1H Pulse with Inverse Spectrometer Configuration11 Experiment - The 90 13C Decoupler Pulse with Inverse Configuration11 Experiment - Composite Pulses12 Experiment - Radiation Damping13 Experiment - Pulse and Receiver Phases13 Experiment - Determination of radiofrequency Power14 CHAPTER 3 - ROUTINE NMR SPECTROSCOPY AND STANDARD TESTS15 SUMMARY15 Experiment - The Standard 1H NMR Experiment15 Experiment - The Standard 13C NMR Experiment16 Experiment - The Application of Window Functions16 E

2.9 zg Determination of Radiofrequency Power Experiment 2.1 - Determination of the 90° 1H Transmitter Pulse Duration pulse program: zg0 1D-sequence, using p0 for any flip angle. Result is a routine proton NMR spectrum. Setting of the needed channels: F1: 1H F2: off Acquisition parameters PL1 : F1 channel - high power level for 1H

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