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加硫したゴムの分析 - customs.go.jp

46 69 * * * Analysis of Vulcanised Rubbers Kenji TAKEMOTO*, Hiroyuki WATANABE* and Fumio NAKAMURA* *Central Customs Laboratory, Ministry of Finance 6-3-5, Kashiwanoha, Kashiwa, Chiba 277-0882 Japan We made various vulcanised rubbers and examined the method to detect the structure of vulcanisation with sulphur. By using solid state 13C nuclear magnetic resonance spectrometry (13C-NMR) and pyrolysis gas chromatography (Py-GC), we detected the structure of vulcanisation with sulphur in natural rubber (NR). And by using raman spectrometry and Py-GC, we detected the structure of vulcanisation with sulphur in styrene-butadiene rubber (SBR).

関税中央分析所報 第46号 71 3.2 ラマン分光法 分以降には、 加硫前後を比較したSBR のラマンスペクトルをFig.4 に示す。

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