Transcription of HYDROCARBONS, HALOGENATED 1003
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HYDROCARBONS, HALOGENATED 1003
HYDROCARBONS, HALOGENATED 1003. Table 1 MW: Table 2 CAS: Table 1 RTECS: Table 1. METHOD: 1003, Issue 3 EVALUATION: PARTIAL Issue 1: 15 February 1984. Issue 3: 15 March 2003. OSHA : See TABLE 1 PROPERTIES: See TABLE 2. NIOSH: See TABLE 1. ACGIH: See TABLE 1. COMPOUNDS: See TABLE 1. (synonyms). SAMPLING MEASUREMENT. SAMPLER: SOLID SORBENT TUBE TECHNIQUE: GAS CHROMATOGRAPHY, FID. (coconut shell charcoal, 100 mg/50 mg). (Lot # 2000) ANALYTE: compounds listed above FLOW RATE: to L/min DESORPTION: 1 mL CS2 , stand 30 min VOL-MIN: Table 3 INJECTION. -MAX: Table 3 VOLUME: 1 L. SHIPMENT: Routine TEMPERATURE: Group A: Inj = 200 C, Det = 250 C ;. 35 C (3 min) to 150 C. SAMPLE (8 C/min). STABILITY: 30 days for all analytes Group B: Inj = 225 C, Det = 250 C.
COLUMN: Group A: capillary, fused silica, 30 m x 0.32-mm ID; 1.80-µm film diphenyl/ dimethyl polysiloxane, Rtx®-502.2 or equivalent. Group B: capillary, fused silica, 30 m x 0.53 - mm ID; 3-µm film 35% diphenyl- 65% dimethyl polysiloxane, Rtx®-35 or equivalent. CALIBRATION: standard solutions of analytes in CS 2 RANGE: see Evaluation of Method
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