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METHOD 5031 VOLATILE, NONPURGEABLE, …

CD-ROM5031 - 1 Revision 0 December 1996 METHOD 5031 volatile , nonpurgeable , water - soluble COMPOUNDS BY AZEOTROPIC AND METHOD describes a procedure for separation of nonpurgeable , water - soluble , andvolatile organic compounds in aqueous samples or leachates from solid matrices using azeotropicdistillation. The appropriate gas chromatographic/mass spectrometric (GC/MS) determinative stepsare found in METHOD 8260. The appropriate gas chromatographic/flame ionization (GC/FID)determinative steps are found in METHOD 8015. This separation METHOD should be used as analternative to METHOD 5030 for compounds that are difficult to purge and trap. METHOD 5031 is usefulin the determination of the following compounds: compound NameCAS alcohol107-18-61-Butanol104-51-8t-Butyl alcohol75-65-0 Crotonaldehyde123-73-91,4-Dioxane123-91- 1 Ethanol64-17-5 Ethyl Acetate141-78-6 Ethylene oxide75-21-8 Isobutyl alcohol78-83-1 Methanol67-56-1 Methyl ethyl ketone78-93-3 Methyl isobutyl ketone108-10-1N-Nitroso-di-n-butylamine9 24-16-3 Paraldehyde123-63-72-Pentanone107-87-92- Picoline109-06-81-Propanol71-23-82-Propa nol67-63-0 Propionitrile107-12-0 Pyridine110-86-1o-Toluidine95-53-4 Chemical Abstract Servic

cd-rom 5031 - 1 revision 0 december 1996 method 5031 volatile, nonpurgeable, water-soluble compounds by azeotropic distillation 1.0 scope and application

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