METHOD 8000D DETERMINATIVE …

SW-846 Update VI 8000D - 1 Revision 5 March 2018 METHOD 8000D DETERMINATIVE CHROMATOGRAPHIC SEPARATIONS Table of Contents SCOPE AND APPLICATION .. 1 SUMMARY OF METHOD .. 6 DEFINITIONS .. 7 INTERFERENCES/CHROMATOGRAPHIC PERFORMANCE .. 7 SAFETY .. 8 EQUIPMENT AND SUPPLIES .. 8 REAGENTS AND STANDARDS .. 12 SAMPLE COLLECTION, PRESERVATION, AND STORAGE .. 12 QUALITY 12 CALIBRATION AND STANDARDIZATION .. 25 PROCEDURE .. 26 DATA ANALYSIS AND CALCULATIONS .. 55 METHOD PERFORMANCE .. 55 POLLUTION PREVENTION .. 55 WASTE MANAGEMENT .. 55 REFERENCES .. 56 TABLES, DIAGRAMS, FLOWCHARTS, AND VALIDATION DATA .. 56 APPENDIX A .. 56 SW-846 is not intended to be an analytical training manual. Therefore, METHOD procedures are written based on the assumption that they will be performed by analysts who are formally trained in at least the basic principles of chemical analysis and in the use of the subject technology. In addition, SW-846 methods in this manual, with the exception of required use for the analysis of METHOD -defined parameters, are intended to be guidance documents.

SW-846 Update VI 8000D- 2 Revision 5 March 2018 1.1 Method 8000 is not a determinative method but instead provides guidance on analytical chromatography and describes calibration and QC requirements common to all

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  Methods, Chromatography, Method 8000d determinative, 8000d, Determinative

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