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METHOD 8000D DETERMINATIVE CHROMATOGRAPHIC …

SW-846 Update VI 8000D - 1 Revision 5 March 2018 METHOD 8000D DETERMINATIVE CHROMATOGRAPHIC SEPARATIONS Table of Contents SCOPE AND APPLICATION .. 1 SUMMARY OF METHOD .. 6 DEFINITIONS .. 7 INTERFERENCES/ CHROMATOGRAPHIC PERFORMANCE .. 7 SAFETY .. 8 EQUIPMENT AND SUPPLIES .. 8 REAGENTS AND STANDARDS .. 12 SAMPLE COLLECTION, PRESERVATION, AND STORAGE .. 12 QUALITY 12 CALIBRATION AND STANDARDIZATION .. 25 PROCEDURE .. 26 DATA ANALYSIS AND CALCULATIONS .. 55 METHOD PERFORMANCE .. 55 POLLUTION PREVENTION .. 55 WASTE MANAGEMENT .. 55 REFERENCES .. 56 TABLES, DIAGRAMS, FLOWCHARTS, AND VALIDATION DATA .. 56 APPENDIX A .. 56 SW-846 is not intended to be an analytical training manual.

PID = Photoionization detector TED = Thermionic emission detector TS/MS = Thermospray mass spectrometry UV = Ultraviolet 1.2 Analytical chromatography is used to separate target analytes from co-extracted interferences in samples. Chromatographic methods can be divided into two major categories: GC and HPLC.

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  Methods, Chromatography, Chromatographic, Photoionization, 8000d, Determinative, Method 8000d determinative chromatographic

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