Transcription of METHOD 8327
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METHOD 8327
SW-846 Update VII 8327- 1 revision 0 July 2021 METHOD 8327 PER- AND POLYFLUOROALKYL SUBSTANCES (PFAS) BY LIQUID CHROMATOGRAPHY/TANDEM MASS SPECTROMETRY (LC/MS/MS) TABLE OF CONTENTS SCOPE AND 2 SUMMARY OF METHOD .. 5 DEFINITIONS .. 5 INTERFERENCES .. 5 SAFETY .. 7 EQUIPMENT AND SUPPLIES .. 7 REAGENTS AND STANDARDS .. 9 SAMPLE COLLECTION, PRESERVATION, AND STORAGE .. 13 QUALITY CONTROL .. 14 CALIBRATION AND STANDARDIZATION .. 20 PROCEDURE .. 20 DATA ANALYSIS AND CALCULATIONS .. 25 METHOD PERFORMANCE .. 26 POLLUTION PREVENTION .. 26 WASTE 26 REFERENCES .. 27 TABLES, DIAGRAMS, FLOW CHARTS, AND VALIDATION DATA .. 28 TABLE 1. RECOVERY AND PRECISION OF TARGET ANALYTES IN MULTI-LABORATORY STUDY MATRICES PREPARED BY METHOD 3512 .. 29 TABLE 2. RECOMMENDED PRECURSOR IONS AND PRODUCT IONS AND EXAMPLE CHROMATOGRAPHIC RETENTION TIMES.
SW-846 Update VII 8327- 4 Revision 0 July 2021 1.1 Prior to employing this method, analysts are advised to consult the base method for each type of procedure that may be employed in the overall analysis (e.g., Methods 3500, 3600 and 8000) for additional information on QC procedures, development of QC acceptance
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