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POLYNUCLEAR AROMATIC HYDROCARBONS by …
NIOSH Manual of Analytical Methods (NMAM), Fourth EditionPOLYNUCLEAR AROMATIC HYDROCARBONS by HPLC5506 Formulae: Table 1MW: Table 1 CAS: Table 2 RTECS: Table 2 METHOD: 5506, Issue 3 EVALUATION: PARTIALI ssue 1: 15 May 1985 Issue 3: 15 January 1998 OSHA :Table 3 NIOSH:Table 3 ACGIH:Table 3 PROPERTIES:Table 1 Compoundsacenaphthenebenzo[ghi]perylenef luoreneacenaphthylenebenzo[a]pyreneinden o[1,2,3-cd]pyreneanthracenebenzo[e]pyren enaphthalenebenz[a]anthracenechrysenephe nanthrenebenzo[b]fluoranthenedibenz[a,h] anthracenepyrenebenzo[k]fluoranthenefluo rantheneNAMES & SYNONYMS:Polycyclic AROMATIC HYDROCARBONS , PAHs; also see Table :FILTER + SORBENT TUBE(37-mm, 2- m, PTFE + washed XAD-2, 100mg/50 mg)FLOW RATE:2 L/minVOL-MIN:200 L -MAX:1000 LSHIPMENT:transfer filters to culture tubes; wrap sorbentand culture tubes in Al foil; ship @ 0 CSAMPLESTABILITY:unknown; protect from heat and UV lightFIELD BLANKS:3 to 10 field blanks per setMEDIA BLANKS:6 to 10 media blanks per setTECHNIQUE: hplc , FLUORESCENCE/UVDETECTIONANALYTE:compound s listed aboveEXTRACTION:5 mL acetonitrile; ultrasonic bath, 30 to 60minutesINJECTIONVOLUME:10 to 50 LMOBILE PHASE:acetonitrile/water gradient @ ambienttemperature, 1 mL/minCOLUMN:250 x , reversed-phase, 5- m C18 DETECTOR:UV @ 254 nm; fluorescence @ 340 nm(excitation), 425 nm (emission)CALIBRATION:standards in acetonitrileRANGE:see EVALUATION OF METHODESTIMATED LOD:see EVALUATION OF METHODPRECISION (r)
POLYNUCLEAR AROMATIC HYDROCARBONS by HPLC: METHOD 5506, Issue 3, dated 15 January 1998 - Page 2 of 9 NIOSH Manual of …
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Chapter 5.9 Polycyclic aromatic hydrocarbons, Polycyclic aromatic hydrocarbons, Polynuclear aromatic hydrocarbons in Drinking, Polynuclear aromatic hydrocarbons in Drinking-water, Hydrocarbons, Aromatic hydrocarbons, HYDROCARBONS, AROMATIC 1501, SAFETY DATA SHEET: AROMATIC 200, Aromatic, SAFETY DATA SHEET: AROMATIC 150, Lecture 15 Oil, Grease, Surfactants, and, Lecture 15 Oil, Grease, Surfactants, and Hydrocarbons, Background Levels of Polycyclic Aromatic