Transcription of Preparation and Characterisation of Metal Acetylacetonate ...
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Preparation and Characterisation of Metal Acetylacetonate ...
RCarbon1 RPreparation and Characterisationof Metal Acetylacetonate ComplexesCarbonRCarbon2 Contents Objectives 3 Introduction 3 Experiment 6 Safety 6 AI3+ Complex 6 Co3+ Complex 8 Mn3+ Complex 10 Fe3+ Complex 13 Cu2+ Complex
(Powerscan = 2 minutes, 40 scans). 31 30 29 28 27 26 25 24 23 22 21 20 19 18 17 16 15 14 13 12 11 10 9 8 7 6 5 4 3 2 1 0-1 f1 (ppm) 7 6 5 4 3 2 1 f1 (ppm) 6. 2 0 0. 9 1 1. 9 9 5. 4 7 7. 2 6 C D C l 3 The 1H-NMR spectrum of Al(acac) 3 (Figure 3) has sharp resonances in the region between 0 – 8 ppm, typical for most molecules.
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