Transcription of Residual Solvent Analysis - Restek
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Residual Solvent Analysis - Restek
Satisfy USP <467> requirements detailed procedures inside. Improve system suitability passrates with an optimized system. Easy technical tips ensure successful Solvent AnalysisImplementing USP <467>Procedure AIdentificationProcedure BConfirmationProcedure CQuantificationPrepare Standardand Test SolutionsPerform Procedure Under Method-Specified Systemand ConditionsResidual SolventsPeaks Present at an Area Greater than theCorrespondingStandard?NONOP asses TestNo Further ActionYESYESP repare Standardand Test SolutionsPerform Procedure Under Method-Specified Systemand ConditionsResidual SolventsPeaks Present at an Area Greater than theCorrespondingStandard?Passes TestNo Further ActionCalculate Amount of Residual solvents PresentOverview of Method The United States Pharmacopeia (USP) general chapter <467> Residual solvents is a widely used compendial method for identifyingand quantifying Residual solvents when no information is available on what solvents are likely to be present.
6 visit www.restek.com/usp467 Achieving USP <467> Compliance (cont.) Procedure B - Confirmation Once a residual solvent is identified and found to be above the percent daily exposure limit, Procedure B
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