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Soil Sample Collection and Analysis Procedures

Soil Sample Collection and Analysis Procedures Petroleum Remediation Program This document describes the Procedures for field screening of petroleum-contaminated soil and Collection of soil samples for laboratory Analysis . The Minnesota Pollution Control Agency (MPCA) Petroleum Remediation Program (PRP) conducts random on- site audits of fieldwork. Give the PRPat least 48 hours' notice prior to conducting fieldwork at sites under program oversight. Find information on the fieldwork notification process at Prior notification of fieldwork is mandatory and will be verified upon submittal of the results.

When methanol is used as the preservative, GRO and VOC results can be obtained from the same sample. Preserve approximately 25 grams of soilwith 25 ml of methanol in a tared 60-ml vial. A ... 1,001-2,000 4 2,001-4,000 5 Each additional 2,000 One additional sample .

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