Acid-Base Extraction
extract with NaOH/H2O UPPER LAYER (ETHER) (ether sol/H2O insol) neutral compound LOWER LAYER (AQUEOUS) (water sol, ether insol) HCl O H (ether sol, water insol) Neutralization of the carboxylic acid salt and excess sodium bicarbonate with concentrated hydrochloric acid. It is critical to add an amount of HCl necessary to completely neutralize ...
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