Appendix I Standard Operating Procedures and Standard ...

1 Appendix I Standard Operating Procedures and Standard quality Procedures This page intentionally left blank Department of Energy Oakland Operations Office, Oakland, California FINAL Standard Operating Procedures for the: Environmental Restoration/Waste Management La boratory for Energy-Related Health Research (LEHR) University of California at Davis, California Prepared for: United States Department of Energy Oakland Operations Office 1301 Clay Street Oakland, California 95612-5208 Prepared by: Weiss Associates 5801 Christie Avenue, Suite 600 Emeryville, CA 94608-1827 DOE Oakland Operations Contract DE-AC03-96SF20686 J:\DOE\4000\D3\SQ&OPS\WASOPS\ WEISS ASSOCIATES Project Number: 128-4000 FINAL Standard Operating Procedures for the: Environmental Restoration/Waste Management La boratory for Energy-Related Health Research (LEHR) University of California at Davis, California Prepared for: United States Department of Energy Oakland Operations Office 1301 Clay Street Oakland, California 95612-5208 Prepared by: Weiss Associates 5801 Christie Avenue, Suite 600 Emeryville, CA 94608-1827 DOE Oakland Operations Contract DE-AC03-96SF20686 Is sued To: _____ Date: _____ Copy No.

2 : _____ Controlled Uncontrolled J:\DOE\4000\D3\SQ&OPS\WASOPS\ WEISS ASSOCIATES Project Number: 128-4000 Approvals Page FINAL Standard Operating Procedures for the: Environmental Restoration/Waste Management La boratory for Energy-Related Health Research (LEHR) University of California at Davis, California Prepared for: United States Department of Energy Oakland Operations Office 1301 Clay Street Oakland, California 95612-5208 Prepared by: Weiss Associates 5801 Christie Avenue, Suite 600 Emeryville, CA 94608-1827 October, 2010 Approved by: Date: Mary Stallard, Project quality Assurance Manager Weiss Associates Approved by: Date: Robert O. Devany, , Project Manager Weiss Associates Approved by: Date: Michael D. Dresen, , Program Manager Weiss Associates Standard Operating Procedures and Forms Table of Contents LEHR Environmental Restoration / Waste Management 12/10/99 DOE Contract No.

3 DE-AC03-96SF20686 Page i of vi J:\DOE\4000\D3\SQ&OPS\WASOPS\ WEISS ASSOCIATES Project Number: 128-4000 TABLE OF CONTENTS AND LOG OF REVISIONS Standard Operating Procedures SOP No. Title Revision No. Date of Revision SOP Chain-of-Custody 1 3/99 SOP Sample Handling, Packaging and Shipping 2 12/99 SOP Surface and Shallow Subsurface Soil Sampling 1 4/02 SOP Subsurface Soil Sampling While Drilling 1 4/02 SOP Compaction of Fill Material 0 3/98 SOP Water Level Measurements in Monitoring Wells 0 3/98 SOP Non-aqueous Phase Liquid Measurement in Monitoring Wells 0 3/98 SOP Sampling Equipment and Well Material Decontamination 0 3/98 SOP Drilling, Development and Heavy Equipment Decontamination 0 3/98 SOP Surface and Subsurface Geophysics 0 3/98 SOP Monitoring Well Installation 0 3/98 SOP Monitoring Well Development 0 3/98 SOP Bore Hole and Well Abandonment 0 3/98 SOP Low Flow Ground Water Sampling with Dedicated Pumps 1 10/10 SOP Soil Organic Vapor Sampling 0 3/98 SOP Cone Penetration Testing and Hydropunch Ground Water Sampling 0 3/98 SOP Sample Collection.

4 Handling and Data Documentation for Field Analysis Using Gamma Spectrometer and Beta Scintillation Dectector 0 6/98 SOP Radium-226 Analysis by Gamma Spectrometer 0 7/01 SOP Strontium-90 Analysis by Beta Scintillation Sensor 3 7/01 SOP Aquifer Testing 0 3/98 SOP Soil Stockpiling 0 3/98 SOP Ambient Air Monitoring 1 3/99 SOP Hollow Stem Auger Drilling 0 3/98 SOP Mud Rotary Drilling 0 3/98 SOP Air Rotary Drilling 0 3/98 SOP Dual Tube Percussion Drilling 0 3/98 SOP Lithologic Logging 0 3/98 SOP Sample Labeling 0 3/98 SOP Sample Numbering 0 3/98 SOP Field QC Sampling 0 3/98 Standard Operating Procedures and Forms Table of Contents LEHR Environmental Restoration / Waste Management 12/10/99 DOE Contract No. DE-AC03-96SF20686 Page ii of vi J:\DOE\4000\D3\SQ&OPS\WASOPS\ WEISS ASSOCIATES Project Number: 128-4000 SOP On-Site Sample Storage 0 3/98 SOP Sample Containers, Preservation, and Holding Times 0 3/98 SOP Data validation 1 10/10 SOP Sample Data Management 0 10/10 SOP Land Surveying 0 3/98 SOP Radiological Areas and Postings[see RPP] 1 3/99 SOP Radiological Surveys and Instrumentation [see RPP] 1 3/99 SOP Radiological Survey Forms (Update 1) [see RPP] 0 7/98 SOP Drum Crusher Operation and Servicing 0 3/98 SOP Taskmaster Heavy Duty Solids Disintegrator (Shredder)

5 Operation and Servicing 0 3/98 SOP Lead Characterization, Packaging and Shipping 0 3/98 SOP Contamination Control [see RPP] 1 3/99 SOP Waste Processing and Packaging 0 7/98 SOP Low-Level Radioactive Waste Storage 0 3/99 SOP Waste Shipment 2 6/01 SOP Clean Waste Handling 0 3/98 SOP Waste Tracking System 0 2/99 SOP Waste Certification 0 3/98 SOP Waste Characterization for Off-Site Shipment 0 6/01 SOP Tennelec Series 5 Low Background Counting System [see RPP] 0 3/99 SOP Liquid Scintillation Counter (LSC) [see RPP] 0 3/99 SOP Check-in and Orientation for Radiological Workers, General Employees and Members of the Public [see RPP] 2 11/99 SOP External Dosimetry Issuance [see RPP] 2 11/99 SOP Radiation Protection Records [see RPP] 2 11/99 SOP Radiological Protection Program Audits [see RPP] 1 3/99 SOP Occupational Exposure Reports [see RPP] 1 3/99 SOP LEHR Site Inspection [see RPP] 1 3/99 SOP Ambient Radiation Monitoring Program 0 4/98 SOP LEHR Document Review Procedures 0 3/98 SOP Environment, Safety and Health Reporting 0 9/01 SOP Security 0 11/01 Standard Operating Procedures and Forms Table of Contents LEHR Environmental Restoration / Waste Management 12/10/99 DOE Contract No.

6 DE-AC03-96SF20686 Page iii of vi J:\DOE\4000\D3\SQ&OPS\WASOPS\ WEISS ASSOCIATES Project Number: 128-4000 FORMS AND FIGURES FOR Standard Operating Procedures SOP No. Form No. Form Title Revision No. Date of Revision SOP Chain-of-Custody Record 1 3/99 Field Activity Daily Log 2 12/99 SOP None SOP Sample Collection Log 1 4/02 SOP Borehole/Well Construction Log 0 3/98 SOP None SOP Water Levels Form 0 3/98 Well Development Data Form 0 3/98 Water Sampling Data Form 0 3/98 SOP None SOP None SOP None SOP None SOP Borehole/Well Construction Log 0 3/98 SOP Well Development Data Form 0 3/98 SOP DWR Form 188, Rev. 7-90 0 3/98 Well Abandonment Log 0 3/98 SOP None SOP None SOP None SOP Field Screening Samples and Analysis Form 0 6/98 SOP None SOP None SOP Example Air Monitoring Chain-of-Custody 0 4/98 Air Sampling Station Meter Log 0 4/98 Radtrack Alpha Track Chain-of-Custody 0 4/98 SOP None SOP None SOP None SOP None SOP Borehole/Well Construction Log 0 3/98 SOP Example Sample Label 0 3/98 Standard Operating Procedures and Forms Table of Contents LEHR Environmental Restoration / Waste Management 12/10/99 DOE Contract No.

7 DE-AC03-96SF20686 Page iv of vi J:\DOE\4000\D3\SQ&OPS\WASOPS\ WEISS ASSOCIATES Project Number: 128-4000 SOP None SOP None SOP None SOP Equipment Checklist 0 3/98 Table 1. Recommendations for Water Samples 0 3/98 Table 2. Recommendations for Sediment/Soil Samples 0 3/98 SOP validation of Organic Data by GC/MS Analysis 1 9/10 validation of Organic Data by GC Analysis 1 9/10 validation of Radiochemistry Data 0 1/98 validation of Metals Data 1 9/10 validation of Data from Wet Chemistry or other Miscellaneous Analyses 0 1/98 Data validation Qualifier Definitions 0 1/98 LEHR Data validation Summary 0 1/98 SOP Data Reporting Form 1/98 SOP standards for Third-Order Plane Surveys 0 3/98 SOP Surface Confirmation Values 0 6/99 Values for Establishing Sealed Radioactive Source Accountability with Radioactive Material Posting and Labeling Requirements 1 6/99 SOP Radiological Survey Log Sheet 1 3/99 SOP Radiological Survey Form 0 7/98 Radiological Survey Form Continuation Sheet 0 7/98 Radiological Survey Log Sheet 1 3/99 Radioactive Airborne Contamination Survey

8 Report Form 0 7/98 Scaler Setup Sheet 0 7/98 Scaler Daily Source Check Sheet 0 7/98 SOP None SOP None SOP None SOP Surface Contamination Values 1 3/99 Guidelines for Contamination Control Practices 1 3/99 Guidelines for Contamination Control Practices 1 3/99 Standard Operating Procedures and Forms Table of Contents LEHR Environmental Restoration / Waste Management 12/10/99 DOE Contract No. DE-AC03-96SF20686 Page v of vi J:\DOE\4000\D3\SQ&OPS\WASOPS\ WEISS ASSOCIATES Project Number: 128-4000 Checklist for Reducing Occupational Radiation Exposure 1 3/99 Physical Access Controls for High and Very High Radiation Areas 1 3/99 Guidelines for Personnel Contamination Monitoring with Hand Held Instruments 1 3/99 SOP Container Log 0 3/98 SOP Waste Management Weekly Inspection Checklist SOP Waste Shipment Checklist 0 7/98 Transport Vehicle Inspection Checklist 0 7/98 Exclusive Use Instructions 0 7/98 Document Package Distribution 0 7/98 SOP Waste/Material Evaluation Process 2 6/01 SOP Example of Waste Tracking Sheet (Form SOP ) 0 2/99 Example of Completed Waste Tracking Sheet 0 2/99 SOP None SOP None SOP None SOP LEHR Visitor Sign-In Log 2 11/99 Visitor Orientation Form 2 11/99 General Employee Radiation Training Log (GERT)

9 2 11/99 Personal/Occupational History 2 11/99 Request for Report of Radiation History 2 11/99 Training Certificate List 2 11/99 SOP None SOP None SOP RPP Audit Plan Schedule 1 3/99 SOP None SOP None SOP Environmental Dosimetry Inspection Form 0 4/98 TLD Locations 0 11/97 SOP QA/QC Checklist for Documents 0 3/98 Document Review Tracking Form 0 3/98 SOP US DOE Individual Accident/Incident Report DOE M Tabulation of Work Hours and Vehicle Usage, and Property Valuation Standard Operating Procedures and Forms Table of Contents LEHR Environmental Restoration / Waste Management 12/10/99 DOE Contract No. DE-AC03-96SF20686 Page vi of vi J:\DOE\4000\D3\SQ&OPS\WASOPS\ WEISS ASSOCIATES Project Number: 128-4000 Transmittal of Individual Accident/Incident Reports OMB Burden Disclosure Statement Instructions for Preparing Occupational Exposure Data Summaries SOP None Note: SOPs and associated forms may be revised, added, or deleted in accordance with the pr ovisions of the quality Assurance Project Plan.

10 SOPs and associated forms are not numbered sequentially. Therefore, a missing number in the above list does not signify that a SOP or associated form is missing. SOPs annotated [see RPP] are not included in this volume, but are included in a separate volume with the Radiological Protection Program (RPP). Final Standard Operating Procedures SOP NO. LEHR Environmental Restoration / Waste Management Rev. 1 3/31/99 DOE Contract No. DE-AC03-96SF20686 Page 1 of 5 J:\DOE_Stoller\4110\330\QAPP\RevB\SOPs_S QPs\SOPs\ Weiss Associates Project Number: 128-4000 CHAIN-OF-CUSTODY Standard Operating PROCEDURE PURPOSE This Standard Operating Procedure (SOP) establishes the method and responsibilities associated with the maintenance and custody of samples which are to be used to provide data which form a basis for making project related decisions. It outlines the general Procedures for maintaining and documenting sample chain of custody from the time of sample collection through sample disposition.