Basic- NMR- Experiments

1 150 Basic- NMR-ExperimentsMMO January 2000 Version 2 - DETERMINATION OF THE PULSE-DURATION9 SUMMARY9 Experiment - Determination of the 90 1H Transmitter Pulse Duration9 Experiment - Determination of the 90 13C Transmitter Pulse Duration10 Experiment - Determination of the 90 1H Decoupler Pulse Duration10 Experiment - The 90 1H Pulse with Inverse Spectrometer Configuration11 Experiment - The 90 13C Decoupler Pulse with Inverse Configuration11 Experiment - Composite Pulses12 Experiment - Radiation Damping13 Experiment - Pulse and Receiver Phases13 Experiment - Determination of Radiofrequency Power14 CHAPTER 3 - ROUTINE NMR SPECTROSCOPY AND STANDARD TESTS15 SUMMARY15 Experiment - The Standard 1H NMR Experiment15 Experiment - The Standard 13C NMR Experiment16 Experiment - The Application of Window Functions16 Experiment - Computer-aided Spectral Analysis17 Experiment - Line-Shape Test for 1H NMR Spectroscopy17 Experiment - Resolution Test for 1H NMR Spectroscopy18 Experiment - Sensitivity Test for 1H NMR Spectroscopy18 Experiment - Line-Shape Test for 13C NMR Spectroscopy19 Experiment - ASTM Sensitivity Test for 13C NMR Spectroscopy20 Experiment - Sensitivity Test for 13C NMR Spectroscopy20 Experiment - Quadrature

2 Image Test21 Experiment - Dynamic Range Test for Signal Amplitudes21 Experiment 13 Phase Stability Test22 CHAPTER 4 - DECOUPLING TECHNIQUES23 SUMMARY23 Experiment - Decoupler Calibration for Homonuclear Decoupling23 Experiment - Decoupler Calibration for Heteronuclear Decoupling243 Experiment - Low Power Calibration for Heteronuclear Decoupling25 Experiment - Homonuclear Decoupling25 Experiment - Homonuclear Decoupling at Two Frequencies26 Experiment - The Homonuclear SPT Experiment26 Experiment - The Heteronuclear SPT Experiment27 Experiment - 1D Nuclear Overhauser Difference Spectroscopy27 Experiment - 1D NOE Spectroscopy with Multiple Selective Irradiation28 Experiment - 1H Off-Resonance Decoupled 13C NMR Spectra29 Experiment - The Gated 1H-Decoupling Technique29 Experiment - The Inverse Gated 1H-Decoupling Technique30 Experiment - 1H Single Frequency Decoupling of 13C NMR Spectra30 Experiment - 1H Low Power Decoupling of 13C NMR Spectra31 Experiment - Measurement of the Heteronuclear Overhauser Effect32 CHAPTER 5 - DYNAMIC NMR SPECTROSCOPY33 SUMMARY33 Experiment - Low Temperature Calibration with Methanol33 Experiment - High Temperature Calibration with 1.

3 2-Ethandiol33 Experiment - Dynamic 1H NMR Spectroscopy on Dimethylformamid34 Experiment - The Saturation Transfer Experiment34 Experiment - Measurement of the Rotating Frame Relaxation Time T1p35 CHAPTER 6 - 1D MULTIPULSE SEQUENCES36 SUMMARY36 Experiment - Measurement of the Spin-Lattice Relaxation Time T136 Experiment - Measurement of the Spin-Spin Relaxation Time T237 Experiment - 13C NMR Spectra with SEFT38 Experiment - 13C NMR Spectra with APT38 Experiment - The Basic INEPT Technique39 Experiment - INEPT+40 Experiment - Refocused INEPT40 Experiment - Reverse INEPT41 Experiment - DEPT-13542 Experiment - Editing 13C NMR Spectra with DEPT42 Experiment - Multiplicity Determination with PENDANT43 Experiment - 1D-INADEQUATE44 Experiment - The BIRD Filter45 Experiment - TANGO454 Experiment - The Heteronuclear Double Quantum Filter46 Experiment - Purging with a Spin-Lock Pulse46 Experiment - Water Suppression by Presaturation47 Experiment - Water Suppression by the Jump and Return Method48 CHAPTER 7 - NMR SPECTROSCOPY WITH SELECTIVE PULSES49 SUMMARY49 Experiment - Determination of a Shaped 90o 1H Transmitter Pulse49 Experiment - Determination of a Shaped 90o 1H Decoupler Pulse50 Experiment - Determination of a

4 Shaped 90o 13C Decoupler Pulse50 Experiment - Selective Excitation with DANTE51 Experiment - SELCOSY52 Experiment - SELINCOR: Selective Inverse H,C Correlation via 1J (C,H)52 Experiment - SELINQUATE53 Experiment - Selective TOCSY54 Experiment - INAPT55 Experiment - Determination of Long-Range C,H coupling Constants56 Experiment - SELRESOLV57 Experiment - SERF57 CHAPTER 8 - AUXILIARY REAGENTS, QUANTITATIVE DETERMINATIONS ANDREACTION MECHANISM59 SUMMARY59 Experiment - Signal Separation Using a Lanthanide Shift Reagent59 Experiment - Signal Separation of Enantiomers Using a Chiral Shift Reagent60 Experiment - Signal Separation of Enantiomers Using a Chiral Solvating Agent60 Experiment - Determination of Enantiomeric Purity with Pirkle s Reagent61 Experiment - Determination of Enantiomeric Purity by 31P NMR61 Experiment - Determination of Absolute Configuration by the Advanced Mosher Method62 Experiment - Aromatic Solvent-Induced Shift (ASIS)

5 62 Experiment - NMR Spectroscopy of OH-Protons and H/D Exchange63 Experiment - Isotope Effects on Chemical Shielding64 Experiment - pKa Determination with 13C NMR64 Experiment - The Relaxation Reagent Cr(acac)365 Experiment - Determination of Paramagnetic Susceptibility by NMR65 Experiment - 1H and 13C NMR of Paramagnetic Compounds66 Experiment - The CIDNP Effect67 Experiment - Quantitative 1H NMR Spectroscopy: Determination of the Alcohol Content ofPolish Vodka675 Experiment - Quantitative 13C NMR Spectroscopy with Inverse Gated 1H-Decoupling68 Experiment - NMR Using Liquid-Crystal Solvents68 CHAPTER 9 - HETERONUCLEAR NMR SPECROSCOPY70 SUMMARY70 Experiment - 1H-Decoupled 15N NMR Spectra with DEPT70 Experiment - 1H-Coupled 15N NMR Spectra with DEPT71 Experiment - 19F NMR Spectroscopy71 Experiment - 29Si NMR Spectroscopy with DEPT72 Experiment - 29Si NMR Spectroscopy with Spin-Lock Polarization73 Experiment - 119Sn NMR Spectroscopy73 Experiment - 2H NMR Spectroscopy74 Experiment - 11B NMR Spectroscopy74 Experiment.

6 17O NMR Spectroscopy with RIDE75 Experiment - 47/49Ti NMR Spectroscopy with ARING76 CHAPTER 10 - THE SECOND DIMENSION77 SUMMARY77 Experiment - 2D J-Resolved 1H NMR Spectroscopy77 Experiment - 2D J-Resolved 13C NMR Spectroscopy78 Experiment - The Basic H,H-COSY-Experiment79 Experiment - Long-Range COSY79 Experiment - Phase-Sensitive COSY80 Experiment - Phase-Sensitive COSY-4581 Experiment - - Double Quantum Filtered COSY with Presaturation82 Experiment - Fully Coupled C,H Correlation (FUCOUP)83 Experiment - C,H Correlation by Polarization Transfer (HETCOR)84 Experiment - Long-Range C,H Correlation by Polarization Transfer85 Experiment - C,H Correlation via Long-Range Couplings (COLOC)

7 86 Experiment - The Basic HMQC Experiment86 Experiment - Phase-Sensitive HMQC with BIRD Filter and GARP Decoupling87 Experiment - Poor Man s Gradient HMQC88 Experiment - Phase-Sensitive HMBC with BIRD Filter89 Experiment - The Basic HSQC Experiment90 Experiment - The HOHAHA or TOCSY Experiment91 Experiment - The NOESY Experiment92 Experiment - The CAMELSPIN or ROESY Experiment936 Experiment - The HOESY Experiment94 Experiment - 2D-INADEQUATE94 Experiment - The EXSY Experiment95 Experiment - X, Y Correlation96 CHAPTER 11 - NMR SPECTROSCOPY WITH PULSED FIELD GRADIENTS98 SUMMARY98 Experiment - Calibration of Pulsed Field Gradients98 Experiment - Gradient Preemphasis99 Experiment - Gradient Amplifier Test99 Experiment - Determination of Pulsed Field Gradient Ring-Down Delays100 Experiment - The Pulsed Gradient Spin-Echo Experiment100 Experiment - Excitation Pattern of Selective Pulses101 Experiment - The Gradient zz-Filter102 Experiment - gs-SELCOSY102 Experiment - gs-SELTOCSY103 Experiment - DPFGSE-NOE104 Experiment - gs-SELINCOR105 Experiment - GRECCO106 Experiment - WATERGATE106 Experiment.

8 Water Suppression by Excitation Sculpting107 CHAPTER 12 - 2D NMR SPECTROSCOPY WITH FIELD GRADIENTS108 SUMMARY108 Experiment - gs-COSY108 Experiment - Phase-Sensitive gs-DQF-COSY109 Experiment - gs-HMQC110 Experiment - gs-HMBC110 Experiment - ACCORD-HMBC111 Experiment - Phase-Sensitive gs-HSQC with Sensitivity Enhancement112 Experiment - gs-TOCSY113 Experiment - gs-HMQC-TOCSY114 Experiment - 2Q-HMBC115 Experiment - Gradient-Selected 1H-Detected 2D INEPT-INADEQUATE116 Experiment - gs-NOESY117 Experiment - gs-HSQC-NOESY118 Experiment - gs-HOESY119 Experiment - 1H, 15N Correlation with gs-HMQC1197 CHAPTER 13 - THE THIRD DIMENSION121 SUMMARY121 Experiment - 3D HMQC-COSY121 Experiment - 3D gs-HSQC-TOCSY122 Experiment - 3D H,C,P-Correlation122 Experiment - 3D HMBC123 CHAPTER 14 - SOLID-STATE NMR SPECTROSCOPY124 SUMMARY124 Experiment - Shimming Solid-State Probe-Heads124 Experiment Adjusting the Magic Angle125 Experiment - Hartmann-Hahn Matching126 Experiment The Basic CP/MAS Experiment127 Experiment - TOSS127 Experiment - SELTICS128 Experiment - Multiplicity Determination in the Solid-State1298.

9 QWURGXFWLRQHere you will find some information about the Bruker pulse programs andparameters, which are needed to repeat the Experiments shown in thebook: 150 and More Basic NMR Experiments written by S. Braun, , S. Berger, VCH Weinheim, you will find the experiment number, followed by the Bruker pulseprogram, the settings of the different channels and a list of the acquisitionand processing number of the chapters are identically with the number of thechapters in the book contains a lot of very interesting Experiments . If you want torepeat such Experiments with a BRUKER Avance instrument you needthe pulse program and the parameters belonging to the pulse needed parameters are sometimes different or more then mentio