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SAMPLE CONTAINER, VOLUMES, PRESERVATIVES, …

SAMPLE container , VOLUMES, PRESERVATIVES, and holding TIMES. GENERAL CHEMISTRY. Analysis Product Code Aqueous Aqueous container preservative Holding Time Notes Minimum Requested volume (ml) volume (ml). Acidity ACD 100 200 P,G Cool, < 6oC 14 Days Alkalinity ALK 100 200 P,G Cool, < 6oC 14 Days Ammonia as P,G H2SO4 to pH <2, 28 Days Nitrogen AMN 20 60 Cool, < 6oC. Ash, Percent P,G Cool, < 6oC Not Regulated (dry basis) ASH 100 100. BOD BOD 500 500 P,G Cool, < 6oC 48 Hours A. Bromide BRO 50 100 P,G Cool, < 6oC 28 Days BTU BTU 10 50 P,G Cool, < 6oC Not Regulated Bicarbonate BICARB 100 200 P,G Cool, < 6oC 14 Days Carbonaceous CBOD 500 500 P,G Cool, < 6oC 48 Hours A. BOD. Carbonate CARB 100 200 P,G Cool, < 6oC 14 Days Carbon Dioxide CO2 100 200 P,G Cool, 4oC Immediate Calcium Hardness CAHRD 50 100 P,G HNO3 to pH <2, 6 Months Cool, < 6oC.

SAMPLE CONTAINER, VOLUMES, PRESERVATIVES, AND HOLDING TIMES . GENERAL CHEMISTRY Analysis Product Code …

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Transcription of SAMPLE CONTAINER, VOLUMES, PRESERVATIVES, …

1 SAMPLE container , VOLUMES, PRESERVATIVES, and holding TIMES. GENERAL CHEMISTRY. Analysis Product Code Aqueous Aqueous container preservative Holding Time Notes Minimum Requested volume (ml) volume (ml). Acidity ACD 100 200 P,G Cool, < 6oC 14 Days Alkalinity ALK 100 200 P,G Cool, < 6oC 14 Days Ammonia as P,G H2SO4 to pH <2, 28 Days Nitrogen AMN 20 60 Cool, < 6oC. Ash, Percent P,G Cool, < 6oC Not Regulated (dry basis) ASH 100 100. BOD BOD 500 500 P,G Cool, < 6oC 48 Hours A. Bromide BRO 50 100 P,G Cool, < 6oC 28 Days BTU BTU 10 50 P,G Cool, < 6oC Not Regulated Bicarbonate BICARB 100 200 P,G Cool, < 6oC 14 Days Carbonaceous CBOD 500 500 P,G Cool, < 6oC 48 Hours A. BOD. Carbonate CARB 100 200 P,G Cool, < 6oC 14 Days Carbon Dioxide CO2 100 200 P,G Cool, 4oC Immediate Calcium Hardness CAHRD 50 100 P,G HNO3 to pH <2, 6 Months Cool, < 6oC.

2 Chloride CHL 50 100 P,G Cool, < 6oC 28 Days Chlorine Demand CLD 50 100 P,G Cool, < 6oC Immediate Corrosivity CORR 50 100 P,G Cool, < 6oC Not Regulated Cyanide CN 20 60 P,G NaOH to pH >12, 14 Days Ascorbic Acid, Cool, < 6oC. Cyanides CNA 100 250 P,G NaOH to pH >12, 14 Days B. Amenable to Ascorbic Acid, Chlorination Cool, < 6oC. Chemical Oxygen COD 10 50 P,G H2SO4 to pH <2, 28 Days Demand Cool, < 6oC. Form: SM050-12 SGS t - NJ: ; MA: ; FL: ; TX: ; CO: ; CA: SAMPLE container , VOLUMES, PRESERVATIVES, and holding TIMES. GENERAL CHEMISTRY. Analysis Product Code Aqueous Aqueous container preservative Holding Time Notes Minimum Requested volume (ml) volume (ml). Soils and solids may be analyzed for the above general chemistry parameters at a general requirement of approximately 100g per analyte collected in one 60ml jar.

3 For a combination of analytes, the SAMPLE may be collected in one 300ml bottle. Color COL 100 100 P,G Cool, < 6oC 48 Hours Corrosivity, CORLI See Notes for Test See Notes for Test See Notes Follow Calculation, Requires TDS, Ca Hardness, Langlier Index Vol. Vol. Preservation for pH, Temp, Alk Tests Listed in Notes Cyanide Reactivity CREAC 50 50 P,G Cool, < 6oC Not Regulated C. CTAS CTAS 50 100 P,G Cool, < 6oC 48 Hours Dissolved Oxygen DO 300 300 G ZHS, Cool, < 6oC Immediate Oxidation- EH 100 100 P,G Cool, < 6oC Not Regulated Reduction Potential (ORP or ReDox). Fluoride F 50 100 P Cool, < 6oC 28 Days Hardness HARD 50 100 P,G H2SO4 or HNO3 to 6 Months pH<2. Ignitability IGN 120 200 P,G Cool, < 6oC Not Regulated MBAS (Anionic MBAS 100 200 P,G Cool, < 6oC 48 Hours Surfactants as).

4 Nitrogen, Nitrate XNO3O 25 50 P,G H2SO4 to pH <2, 28 Days E. only Cool, < 6oC. Nitrate + Nitrite NO3 25 50 P,G H2SO4 to pH <2, 28 Days E. Combined Cool, < 6oC. Nitrogen, Nitrite NO2 25 50 P,G Cool, < 6oC 48 hours March 2017 Page 2. SAMPLE container , VOLUMES, PRESERVATIVES, and holding TIMES. GENERAL CHEMISTRY. Analysis Product Code Aqueous Aqueous container preservative Holding Time Notes Minimum Requested volume (ml) volume (ml). Nitrogen, Organic TON (TKN,AMN) (20, 20) (50, 50) P,G H2SO4 to pH<2, M. (TKN AMN) Cool, < 6oC 28 Days Nitrogen, Total TNIT (20, 25) (50, 50) P,G H2SO4 to pH <2, 28 Days N. (TKN + NO32) (TKN + NO32) Cool, < 6oC. Soils and solids may be analyzed for the above general chemistry parameters at a general requirement of approximately 100g per analyte collected in one 60ml jar.

5 For a combination of analytes, the SAMPLE may be collected in one 300ml bottle. Oil & Grease OG1664 1000 2 x 1000 G HCl to pH <2, 28 Days HEM Cool, < 6oC. (Method 1664). Orthophosphate OPO4 50 100 P,G Cool, < 6oC 48 Hours Tetraethyl Lead PBET4 100 500 P ZHS, Cool, < 6oC Not Regulated Paint Filter Test PNTFIL 100 200 P,G Cool, < 6oC Not Regulated Particulate Matter PARMAT 100 200 P,G Cool, < 6oC 7 Days pH by Electrode PH 50 100 P,G Cool, < 6oC Immediate Phenols PN 950 950 G H2SO4 to pH <2, 28 Days A. Cool, < 6oC. Silica, Dissolved SIL 50 100 P Cool, < 6oC 28 Days Specific SCON 125 200 P,G Cool, < 6oC 28 Days Conductance Specific Gravity SG 100 100 P,G Cool, < 6oC Not Regulated Sulfide S 2 X 200 2 x 250 P,G NaOH to pH >12, 7 Days Two (2) Containers Low Level Sulfide SULFLL 2 x 1000 Zinc Acetate, Minimum Cool, < 6oC.

6 Total Chlorine TCHL 5 50 P,G Cool, < 6oC Not Regulated Total Dissolved TDS 200 200 P,G Cool, < 6oC 7 Days March 2017 Page 3. SAMPLE container , VOLUMES, PRESERVATIVES, and holding TIMES. GENERAL CHEMISTRY. Analysis Product Code Aqueous Aqueous container preservative Holding Time Notes Minimum Requested volume (ml) volume (ml). Solids Total Kjeldahl TKN 20 50 P,G H2SO4 to pH <2, 28 Days Nitrogen Cool, < 6oC. Total Mineral TMS 200 200 P,G Cool, < 6oC 7 Days Solids Nitrogen, Nitrite NO2 50 50 P,G Cool, < 6oC 48 Hours Soils and solids may be analyzed for the above general chemistry parameters at a general requirement of approximately 100g per analyte collected in one 60ml jar. For a combination of analytes, the SAMPLE may be collected in one 300ml bottle.

7 Total and/or TOC/DOC 50 60 P,G HCl to pH <2, 28 Days Dissolved Organic Cool, < 6oC. Carbon Total Organic TOCHL 75 100 P,G Cool, < 6oC Not Regulated Chlorine Total Organic TOX (3) 60 (3) 300 G ZHS, H2SO4 to pH 28 Days A. Halides < 2, Cool, < 6oC. Total Phosphates TPO4 100 200 P,G H2SO4 to pH <2, 28 Days Cool, < 6oC. Total Residual TRC 100 200 P,G ZHS, Cool, < 6oC Immediate A. Chlorine Total Solids TS 200 100 P,G Cool, < 6oC 7 Days Total Suspended TSS 1000 (2) 1000 P,G Cool, < 6oC 7 Days F. Solids Turbidity TURB 50 50 P,G Cool, < 6oC 48 Hours Total Volatile TVS 100 100 P,G Cool, < 6oC 7 Days See Total Solids March 2017 Page 4. SAMPLE container , VOLUMES, PRESERVATIVES, and holding TIMES. GENERAL CHEMISTRY. Analysis Product Code Aqueous Aqueous container preservative Holding Time Notes Minimum Requested volume (ml) volume (ml).

8 Solids Total Volatile VSS 1000 (2) 1000 P,G Cool, < 6oC 7 Days See Suspended Suspended Solids Solids Total Mineral TMS 100 100 P,G Cool, < 6oC 7 Days See Total Solids Solids Viscosity VISC 100 100 P,G Cool, < 6oC Not Regulated Soils and solids may be analyzed for the above general chemistry parameters at a general requirement of approximately 100g per analyte collected in one 60ml jar. For a combination of analytes, the SAMPLE may be collected in one 300ml bottle. March 2017 Page 5. SAMPLE container , VOLUMES, PRESERVATIVES, and holding TIMES. MICROBIOLOGY. Analysis Product Code Aqueous Aqueous container preservative Holding Time Notes Minimum Requested volume (ml) volume (ml). Total Coliform TCFC 125 125 P,G,Sterile Na2S2O3, 30 Hour Potable H.

9 (Colilert Method) Cool, < 6oC. Total Coliform TCF 125 125 P,G,Sterile Na2S2O3, 30 Hour Potable, H. (Plate Count Cool, < 6oC 6 Hour Non- Method) Potable Fecal Coliform FCF 125 125 P,G,Sterile Na2S2O3, 6 Hour H. Cool, < 6oC. Total Plate Count TPC 125 125 P,G,Sterile Cool, < 6oC 8 Hour Recom. H. 24 Hour Max. General Petroleum GPD 125 125 P,G,Sterile Cool, < 6oC 24 Hour H. Degraders Recommended Soils and solids may be analyzed for the above Microbiology parameters at a general requirement of approximately 100gm of SAMPLE per analyte collected in one 60ml jar. March 2017 Page 6. SAMPLE container , VOLUMES, PRESERVATIVES, and holding TIMES. METALS AND MINERALS. Analysis Product Code Aqueous Aqueous container preservative Holding Time Notes Minimum Requested volume (ml) volume (ml).

10 Chromium, XCR 100 500 P Cool, < 6oC 24 Hours Hexavalent Iron, Ferrous FE2 100 500 2ml HCL per 100ml Immediate Smp, Cool, < 6oC. Iron, Ferric FE3 * * * * * *D. Lead, Tetraethyl PBET4 100 500 P ZHS, Cool, < 6oC Not Regulated Mercury in Drinking HG 500 500 P HNO3 to pH <2 28 Days Water Low Level Mercury LLHG 2 X 60 500 P HCL within 48hrs 90 Days **. of collection Total Metals Listed per Analyte 500 500 P HNO3 to pH <2 6 Months (aqueous). Cool, < 6oC. (soil and solids). Dissolved Metals Listed per Analyte 500 500 P HNO3 to pH <2 6 Months Wipes for Metals Wipes for Metals 3 X3 gauze pads 3 X3 gauze pads 60 ml vial Cool, < 6oC 6 Months A. Soils and solids may be analyzed for the above metals and minerals at a general requirement of approximately 30gm per analyte collected in one 60ml jar.


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