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Interpreting DSC Data - UC Santa Barbara

Interpreting DSC data TEMPO LABS, MATERIALS RESEARCH LABORATORY UCSB Written by Burton Sickler Interpreting DSC data 1 Table of Contents ANATOMY OF A PEAK .. 2 USING 2 IDENTIFYING TRANSITION EVENTS .. 2 SPLITTING A CURVE INTO SEGMENTS .. 3 SELECTING & HIDING SEGMENTS .. 3 SPLINING SEGMENTS .. 4 CHANGING TO A TEMPERATURE X-AXIS .. 5 IDENTIFYING THE EVENT ONSET 5 IDENTIFYING THE EVENT ENDSET TEMPERATURE .. 5 USING MANUAL SELECT .. 6 RECRYSTALLIZATION EVENTS .. 7 MELTING POINT PEAKS .. 8 MULTIPLE MELTING POINT PEAKS .. 8 POLYMORPHISM .. 9 OVERLAPPING PEAKS .. 9 RECRYSTALLIZATION POINT PEAKS.

Interpreting DSC Data 2 Anatomy of a Peak A DSC event peak typically contains the following components: • Baseline: This is the expected signal (or change in signal) if no transition event occurs (e.g. if the enthalpy change of melting or H

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