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Method 21 8/3/2017 - EPA

Method 21 8/3/ 2017 1 While we have taken steps to ensure the accuracy of this Internet version of the document, it is not the official version. To see a complete version including any recent edits, visit: and search under Title 40, Protection of Environment. Method 21 - DETERMINATION OF VOLATILE ORGANIC COMPOUND LEAKS Scope and Application Analytes. Analyte CAS No. Volatile Organic Compounds (VOC) No CAS number assigned. Scope. This Method is applicable for the determination of VOC leaks from process equipment. These sources include, but are not limited to, valves, flanges and other connections, pumps and compressors, pressure relief devices, process drains, open-ended valves, pump and compressor seal system degassing vents, accumulator vessel vents, agitator seals, and access door seals. Data Quality Objectives. Adherence to the requirements of this Method will enhance the quality of the data obtained from air pollutant sampling methods .

8.1 Instrument Performance Evaluation. Assemble and start up the instrument according to the manufacturer's instructions for recommended warm-up period and preliminary adjustments. 8.1.1 Response Factor. A response factor must be determined for each compound that is to be measured, either by testing or from reference sources.

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