Transcription of RESEARCH PRODUCTS NMR Solvent Data Chart
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LThe 1H spectra of the residual protons and 13C spectrawere obtained on a Varian Gemini 200 spectrometerat 295 K. The NMR solvents used to acquire thesespectra contain a maximum of and TMS(v/v) respectively. Since deuterium has a spin of 1,triplets arising from coupling to deuterium have theintensity ratio of 1:1:1. m denotes a broad peak withsome fine structures. It should be noted that chemicalshifts can be dependent on Solvent , concentrationand values only, may vary with pH, concen-tration and and boiling points are those of the corre-sponding unlabeled compound (except for D2O).These temperature limits can be used as a guide todetermine the useful liquid range of the gathered from the Merck Index Fourteenth Edition. *HOD Peaks - NMR spectra of neat deuterated Solvent always exhibit a peak due to H20 in addition to the residual Solvent peak.
The 1H spectra of the residual protons and 13C spectra were obtained on a Varian Gemini 200 spectrometer at 295°K. The NMR solvents used to acquirethese
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Basic concepts for two-dimensional NMR, 13C NMR, Measuring 13C NMR Spectra, 400 and 500 Using Topspin, NMR yields, Returned To Sender 2005: No Mail Receptacle, Chapter 13: Nuclear Magnetic Resonance (NMR), Chapter 13: Nuclear Magnetic Resonance (NMR) Spectroscopy, Simplified Table of C-13 NMR Chemical Shifts